Single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber and preparation method thereof

A chalcogenide glass and double-clad technology, which is applied in the direction of clad optical fiber, glass optical fiber, glass manufacturing equipment, etc., can solve the problems of poor bonding of the core-clad joint surface, poor surface smoothness, and restrictions on the application of optical fibers, etc., to achieve The roundness is maintained well, the interface is tightly bonded, and the process is operable.

Active Publication Date: 2018-11-02
XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI
View PDF5 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

A single-mode chalcogenide fiber with good performance can be prepared by the double crucible method, but it is generally limited to the preparation of binary system chalcogenide glasses, such as As 2 S 3 、As 2 Se 3 Wait
As for the rod-tube method, the casing is generally obtained by the drilling method at present, and the casing obtained by this method is difficult to be polished, making its surface smoothness poor, which will greatly increase the transmission loss of the optical fiber, and then limit the optical fiber. Applications
In addition, there are still many technical difficulties in the preparation of rare earth-doped single-mode double-clad optical fibers: such as the core-clad is easy to eccentric, the core-clad size ratio is not easy to be quantitatively controlled, and the core-clad bonding surface is not tightly bonded, etc.

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber and preparation method thereof
  • Single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber and preparation method thereof
  • Single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber and preparation method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 2

[0049] The composition of Example 2 is shown in Table 1. Compared with the components of Example 1, corresponding adjustments have been made. The high-speed coil speed is 800 rpm, the coil temperature is 800°C, and the coil time is 1 minute. The melting temperature of the melt quenching method is 900°C, and the quenching time is 0.5 minutes; the specific manufacturing process is the same as in Example 1, and finally a single-mode double-clad dysprosium-doped chalcogenide glass with a diameter of 125 μm is prepared by the hot drawing method optical fiber.

Embodiment 3

[0050] The composition of Example 3 is shown in Table 1. Compared with the components of Examples 1 and 2, corresponding adjustments have been made. The high-speed coil speed is 1000 rpm, the coil temperature is 900 ° C, and the coil time is 2 Minutes, the melting temperature of the melt quenching method is 1000 ° C, and the quenching time is 1 minute; the specific process is the same as that of Examples 1 and 2, and finally a single-mode double-clad composite with a diameter of 150 μm is prepared by the hot drawing method. Dysprosium chalcogenide glass fiber.

[0051] Steps 2)-5) of the present invention mainly include 4 thermal drawing processes and 3 rod and tube combination processes, wherein the first thermal drawing process is to obtain the outer cladding tube and inner cladding tube obtained in the above step 1). and the mandrel are drawn into smaller thin tubes (rods); the first rod tube combination process is to combine the inner clad thin tubes and thin mandrels obta...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

PUM

PropertyMeasurementUnit
Diameteraaaaaaaaaa
Diameteraaaaaaaaaa
Login to view more

Abstract

The invention provides a single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber and a preparation method thereof. The single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber is composed of an outer cladding, an inner cladding and a fiber core. An outer cladding tube and an inner cladding tube are prepared by adopting a high-speed tube rotating method, acore rod is prepared by adopting a melt quenching method, the single-mode double-cladding dysprosium-doped chalcogenide glass optical fiber with small core cladding eccentricity, tight interface adherence, smooth surface and good roundness is prepared by combining with a repeated rod-in-tube method, intermediate infrared optical fiber fluorescence spectra with wavelengths of 2957 and 4258 nm respectively are obtained in later tests, and the optical fiber provided by the invention can be expected to be an ideal intermediate infrared active optical fiber material. The optical fiber preparationmethod solves the problems that the core cladding is prone to be eccentric, the size of the core cladding is not easy to be control quantitatively and the core cladding junction surface is not tightlyattached in the preparation of the existing chalcogenide glass optical fiber.

Description

technical field [0001] The invention relates to the field of optical fiber preparation, in particular to a single-mode double-clad chalcogenide glass optical fiber and a preparation method thereof. Background technique [0002] Compared with oxide and fluoride glasses, chalcogenide matrix glasses have lower maximum phonon energy (300-450cm -1 ), and the low phonon energy is beneficial to reduce the multiphonon relaxation rate of rare earth ions in the process of mid-infrared luminescence transition, which promotes the generation of mid-infrared luminescence. So far, chalcogenide glass optical fiber is the only substrate whose fluorescence emission above 4 μm is observed at room temperature. Therefore, rare earth ion-doped chalcogenide glass fiber is considered to be the most potential matrix material for mid-infrared fiber lasers and amplifiers, and dysprosium-doped chalcogenide glass fiber has an important application prospect in the field of 4-micron fiber lasers. [000...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to view more

Application Information

Patent Timeline
no application Login to view more
IPC IPC(8): G02B6/036G02B6/02C03C13/04C03B37/025
CPCC03B37/025C03C13/043G02B6/02395G02B6/03622
Inventor 郭海涛肖旭升彭波许彦涛陆敏
Owner XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products