Application of flos paulowniae extract in cigarette
A technology of paulownia flower and extract, which is applied in the field of tobacco processing and achieves the effects of stable properties, no toxic and side effects, and low energy consumption
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Embodiment 1
[0014] The application of Paulownia flower extract in cigarettes is specifically:
[0015] Put the fresh paulownia flowers into a constant temperature vacuum oven at 60°C and fully dry them, then cool them naturally in the oven, and take them out. Weigh 100g, pulverize it with a grinder, add it to a 1000 mL round bottom flask, add 375 mL 95% ethanol and 375 mL petroleum ether, heat and reflux in a water bath for 6 h, stop heating, filter while hot, and filter the residue with 95% The mixed solvent of ethanol and petroleum ether (volume ratio 1:1) was washed three times. After the filtrate was cooled, the solvent was evaporated under reduced pressure to obtain a light red viscous liquid, namely natural Paulownia flower extract.
Embodiment 2
[0017] The application of Paulownia flower extract in cigarettes is specifically:
[0018] Put the fresh paulownia flowers into a constant temperature vacuum oven at 60°C and fully dry them, then cool them naturally in the oven, and take them out. Weigh 100g, grind it into a 1000mL round-bottomed flask, add 750mL of petroleum ether, heat and reflux in a water bath for 4 hours, stop heating, filter while hot, wash the residue with petroleum ether three times, and decompress the filtrate after cooling The solvent is evaporated to obtain a light red viscous liquid, which is the natural Paulownia flower extract.
Embodiment 3
[0020] Put the fresh paulownia flowers into a constant temperature vacuum oven at 60°C and fully dry them, then cool them naturally in the oven, and take them out. Weigh 100g, crush it by grinding, add it to a 1000mL round bottom flask, add 750mL 95% ethanol, heat and reflux in a water bath for 7h, stop heating, filter while hot, wash the residue three times with 95% ethanol, and cool the filtrate , and evaporate the solvent under reduced pressure to obtain a light red viscous liquid, that is, the natural Paulownia flower extract.
[0021] Composition analysis of the tobacco spices (extract) prepared in the above examples: Agilent 7890A-5975C GC / MS (Agilent Technologies Co., Ltd., USA) and 400 nuclear magnetic resonance spectrometer (Varian Corporation, USA) were used to analyze and find that The main ingredients are: glucoside, quercetin, kaempferol, high eriodiction, 4,5,7-trihydroxy-3-methoxyflavone, 5-hydroxy-3,4,7-trimethoxy Flavonone, luteolin, acetin, benzaldehyde, van...
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