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Method for separating diamond mixture

A mixture and diamond technology, which is applied in the field of separation and purification of diamond mixture, can solve environmental pollution and other problems, and achieve the effects of high extraction efficiency, good economic benefits, and high purity

Inactive Publication Date: 2018-11-23
辽宁新瑞碳材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional diamond extraction methods use aqua regia or other chemical reagents to remove graphite and catalysts, or use carbon monoxide for chemical reactions to remove metal catalysts. These methods use chemical reagents, which will cause environmental pollution.

Method used

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  • Method for separating diamond mixture

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0062] The invention provides a method for separating diamond mixture, as attached figure 1 shown, including the following steps:

[0063] 1) The mixed material containing iron-cobalt-nickel catalyst, graphite and diamond is sheared and compounded by a squeeze crusher with a shearing function to obtain a material with a particle size of less than 3.0mm; then it is ground by a milling machine, A dissociated and finer-grained ground mixture was obtained with a material content of 70% of particle size -0.074 mm. Among them, the small bat medium, the large wood medium, and the water medium are added to the mill; the ratio of the small bat medium to the large wood medium is 1:2.

[0064] 2) Pass the pulverized mixed material through a hydrodynamic ultrasonic dispersing device for 9 cycles of ultrasonic dispersion treatment to obtain a fully dispersed ultrasonic dispersion mixture.

[0065] 3) The ultrasonic dispersion mixture is first subjected to magnetic separation by a weak ma...

Embodiment 2

[0069] A method for separating a diamond mixture, comprising the steps of:

[0070] 1) The mixed material containing iron-cobalt-nickel catalyst, graphite and diamond is sheared and compounded by a squeeze crusher with a shearing function to obtain a material with a particle size of less than 2.0mm; then it is ground by a milling machine, A dissociated and finer-grained ground mixture was obtained with a material content of -0.074 mm of 80%. Among them, the small bat medium, the large wood medium, and the water medium are added to the mill; the ratio of the small bat medium to the large wood medium is 1:1.

[0071] 2) Pass the pulverized mixed material through a hydrodynamic ultrasonic dispersing device for 11 cycles of ultrasonic dispersion treatment to obtain a fully dispersed ultrasonic dispersion mixture.

[0072] 3) The ultrasonic dispersion mixture is first subjected to magnetic separation by a weak magnetic separator with a magnetic field strength of 120mT to remove th...

Embodiment 3

[0076] A method for separating a diamond mixture, comprising the steps of:

[0077] 1) The mixed material containing iron-cobalt-nickel catalyst, graphite and diamond is sheared and compounded by a squeeze crusher with a shearing function to obtain a material with a particle size of less than 1.5mm; then it is ground by a milling machine, A dissociated and finer-grained ground mixture was obtained with a material content of -0.074 mm of 80%. Among them, the small bat medium, the large wood medium, and the alcohol medium are added to the mill; the ratio of the small bat medium to the large wood medium is 1:2.

[0078] 2) Pass the pulverized mixed material through a hydrodynamic ultrasonic dispersing device for 13 cycles of ultrasonic dispersion treatment to obtain a fully dispersed ultrasonic dispersion mixture.

[0079] 3) The ultrasonic dispersion mixture is first subjected to magnetic separation by a weak magnetic separator with a magnetic field strength of 160mT to remove ...

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Abstract

The invention relates to a method for separating a diamond mixture. The method comprises the following steps that (1) mixed raw materials containing diamond, graphite and an iron-cobalt-nickel catalyst are smashed to obtain a smashed mixture; (2) the smashed mixture is subjected to ultrasonic wave dispersed processing to obtain an ultrasonic wave dispersed mixture; (3) the ultrasonic wave dispersed mixture is subjected to magnetic separation, an iron-cobalt-nickel catalyst product is removed, and a diamond and graphite mixture is obtained; (4) the diamond and graphite mixture is subjected to ultrasonic wave dispersed processing to obtain a dispersed diamond and graphite mixture; and (5) the dispersed diamond and graphite mixture is subjected to staged separation, so that diamond and graphite are separated. Compared with a traditional diamond mixture separating method, the method for separating the diamond mixture is clean and environment-friendly, no chemical reagent is used in the separating process, environmental pollution cannot be caused, and discharge of the three wastes is avoided. The diamond, the graphite and the iron-cobalt-nickel catalyst are respectively separated, so that the purity is high; the graphite and the catalyst matter can be recycled to be reused; and the diamond extraction efficiency is high, and the economic returns are good.

Description

technical field [0001] The invention belongs to the field of separation and purification of diamond mixtures, and in particular relates to a method for separating diamond mixtures. The diamond mixture is dispersed into fine particles, and then diamond, graphite, and iron-cobalt-nickel catalyst products are phase-separated. Background technique [0002] Diamond, commonly known as "diamond", is an allotrope of carbon, and it is the hardest substance naturally occurring in nature. Graphite is also a crystalline mineral of carbonaceous elements, and its crystalline framework is a hexagonal layered structure. Both diamond and graphite are minerals composed of carbon, and the physical and chemical properties of elemental carbon depend on its crystal structure. High-hardness diamond and soft and smooth graphite have different crystal structures, and their appearance, density, melting point, and use are all different. Diamonds are used in a wide range of applications, such as: geo...

Claims

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Application Information

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IPC IPC(8): B03B7/00B03B9/00
CPCB03B7/00B03B9/00
Inventor 孙飞罗立群田金星
Owner 辽宁新瑞碳材料科技有限公司
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