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A barium sulfate particle size control device and method

A particle size control, barium sulfate technology, applied in chemical instruments and methods, calcium/strontium/barium sulfate, calcium/strontium/barium compounds, etc., can solve the problem of low added value, difficult to control particle size distribution, and difficult to achieve artificial interventions to improve productivity

Active Publication Date: 2021-01-12
ZHUSHAN COUNTY QINBA BARIUMSALT CO LTD
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] For a long time, the domestic production of barium sulfate has adopted intermittent manual feeding operation, and the feeding state of the material in the compounding tank is a changing process, so the particle size distribution is difficult to control, and the particle size is different, and it is difficult to achieve human intervention
Therefore, barium sulfate in my country usually has a particle size of about 0.7-1.2 μm, and the particle size is wide. It can only be used as a low-end basic use, which greatly restricts the application and expansion of barium sulfate, and the added value is very low.

Method used

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  • A barium sulfate particle size control device and method
  • A barium sulfate particle size control device and method
  • A barium sulfate particle size control device and method

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0081] 1. The concentration of barium sulfide solution is 170g / L, and the concentration of sodium sulfate solution is 290g / L. at 20m 3 capacity of the reaction tank. Stirring speed 32 rpm;

[0082] 2. The dimensions of the vertical baffle tank 8 used are as follows: the diameter of the vertical baffle tube is 150 mm, the width of the baffle tank 81 is 100 mm, the number of layers is 4, and the distance between the baffle tanks 81 is 120 mm;

[0083] 3. Open the feeding valves of barium sulfide solution and sodium sulfate solution, and feed into the vertical baffle tank 8 at the same time, the flow rate of barium sulfide solution is 7.5m 3 / h, sodium sulfate flow rate 4.1m 3 / h, when feeding to 3 / 4 of the volume of the compounding tank, get the slurry to filter, and use sodium sulfate and barium chloride detection reagents to see if the end of the reaction is reached. Thereafter, close the excess raw material valve, replenish the missing raw material until the end of the re...

Embodiment 2

[0086] 1. The concentration of barium sulfide solution is 175g / L, and the concentration of sodium sulfate solution is 300g / L. 3 Carry out in the reaction tank of volume, stirring speed 32 rev / mins;

[0087] 2. The size of the feeder used is as follows: the diameter of the vertical baffle tube is 150mm, the width of the baffle groove 81 is 100mm, the number of layers is 4, and the distance between the baffles is 120mm. Only sodium sulfate flows through this equipment, and the barium sulfide feeder pipe 15. The diameter is 80mm, straight pipe cutting, no other parts;

[0088] 3. Open the feeding valve of barium sulfide solution and sodium sulfate solution, the flow rate of barium sulfide solution is 8m 3 / h, sodium sulfate flow rate 4.2m 3 / h, when feeding to 3 / 4 of the volume of the compound tank, take the slurry to filter, use sodium sulfate and barium chloride to detect whether the reaction end point is reached, thereafter, close the excess raw material valve, supplement th...

Embodiment 3

[0091] 1. The concentration of barium sulfide solution is 180g / L, and the concentration of sodium sulfate solution is 280g / L. 3 Carry out in the reaction tank of volume, stirring speed 32 rev / mins;

[0092] 2. The size of the feeder used is as follows:

[0093] Ring feeding tube for barium sulfide solution: ring diameter 2.1m, tube diameter 80mm, number of falling water holes 8, hole diameter 20mm;

[0094] Sodium sulfate solution annular feeding pipe: the ring diameter is 1.2m, the pipe diameter is 65mm, the number of falling water holes is 4, and the hole diameter is 20mm;

[0095] 3. Open the feeding valves of barium sulfide solution and sodium sulfate solution, and feed into the annular feeding pipe at the same time, the flow rate of barium sulfide solution is 7.5m 3 / h, sodium sulfate flow rate 3.8m 3 / h, when feeding to 3 / 4 of the volume of the compound tank, take the slurry to filter, use sodium sulfate and barium chloride to detect whether the reaction end point is r...

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Abstract

The invention relates to a barium sulfate grain diameter control device. The barium sulfate grain diameter control device comprises a curing reaction tank, wherein a material distribution device is arranged at the upper end of the curing reaction tank; a feeding pipe communicated with the material distribution device is arranged above the material distribution device; a first solenoid valve, a second solenoid valve, a third solenoid valve, a fourth solenoid valve and a fifth solenoid valve are connected with a control system respectively to connect reaction systems of different grain diameters. A barium sulfate grain diameter control method is realized based on the barium sulfate grain diameter control device; reactions with different diameters are realized through controlling the openingand closing of the solenoid valves; pipe diameters are selected through setting different parameters, and different reaction systems are obtained through the controlling of the solenoid valves; corresponding flow mixing devices are arranged in the corresponding reaction systems and reaction time is controlled, so that barium sulfate with needed grain diameter sizes is obtained through automatically selecting the different reaction systems, and the production rate of automatic reaction is improved.

Description

technical field [0001] The invention relates to the field of chemical production, in particular to a barium sulfate particle size control device and method. Background technique [0002] The particle size of barium sulfate is an extremely important technology in the production of barium sulfate. In barium sulfate market applications, particle size has a significant impact on product dispersibility, color, product transparency and viscosity of the application system. The particle size is required to be less than 0.4 μm in the production of transparent plastics, the particle size of barium sulfate is required to be 0.6-0.7 μm in high-gloss plastic applications, and the particle size is required to be 0.8-1.0 μm in powder coatings and paints. Secondly, the distribution of particle size is also very important, and a narrow particle size distribution is the basic requirement. [0003] For a long time, the domestic production of barium sulfate has adopted intermittent manual fee...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C01F11/46
CPCC01F11/462C01P2004/62
Inventor 赵卓成李盛龙付荣华赵国旗彭斌
Owner ZHUSHAN COUNTY QINBA BARIUMSALT CO LTD