Fibrilia biological dyeing technology based on laccase catalytic polymerization reaction

A technology of biological dyeing and catalytic polymerization, applied in the field of hemp fiber dyeing, can solve the problems of poor rubbing fastness, complex dyeing process, and high requirements for dyeing conditions, and achieve the effects of improving color fixing effect, dyeing efficiency, and dyeing effect.

Inactive Publication Date: 2018-12-11
南通霆川电子科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Traditional dyeing methods and theories based on small molecule synthetic dyes face many challenges, mainly reflected in: complex preparation process of synthetic dyes, large environmental pollution; high requirements for dyeing conditions (often requiring harsh pH value and high temperature), complex dyeing process, and water consumption. High energy consumption and difficult treatment of dyeing wastewater
Commonly used dyes have low molecular weight, dyed products have poor rubbing fastness, low tinting strength, low dye utilization rate, light resistance and heat resistance are also problematic to varying degrees, and fiber applicability is poor, etc.
The natural dyes that have emerged in recent years have been greatly limited in practical application due to incomplete chromatograms, environmental pollution using heavy metal mordants, and poor color fastness.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0025] The present invention provides following technical scheme, a kind of hemp fiber biological dyeing process based on laccase-catalyzed polymerization reaction, comprises the following steps:

[0026] A, hemp fiber is carried out singeing;

[0027] B. Immerse the hemp fiber after singeing in alkaline solution to remove surface impurities and residual pulp;

[0028] C, the hemp fiber after the alkali treatment is put into clear water and repeatedly rinses and puts into the low-temperature drying box to dry;

[0029] D, the hemp fiber after the dry treatment is immersed in the buffer solution containing phenolic monomer and laccase to carry out biological staining;

[0030] E, the hemp fiber after biological dyeing is carried out color fixation, steam processing;

[0031] F, carry out soaping and washing with the hemp fiber at last.

[0032] In this embodiment, the singeing treatment method in step A is: use a heat shield to press the hemp fiber, and then slide back and f...

Embodiment 2

[0041] A kind of biological dyeing process of hemp fiber based on laccase-catalyzed polymerization, comprises the following steps:

[0042] A, hemp fiber is carried out singeing;

[0043] B. Immerse the hemp fiber after singeing in alkaline solution to remove surface impurities and residual pulp;

[0044] C, the hemp fiber after the alkali treatment is put into clear water and repeatedly rinses and puts into the low-temperature drying box to dry;

[0045] D, the hemp fiber after the dry treatment is immersed in the buffer solution containing phenolic monomer and laccase to carry out biological staining;

[0046] E, the hemp fiber after biological dyeing is carried out color fixation, steam processing;

[0047] F, carry out soaping and washing with the hemp fiber at last.

[0048] In this embodiment, the singeing treatment method in step A is: use a heat shield to press the hemp fiber, and then slide back and forth on the heated metal surface for 5 seconds.

[0049] In this...

Embodiment 3

[0057] A kind of biological dyeing process of hemp fiber based on laccase-catalyzed polymerization, comprises the following steps:

[0058] A, hemp fiber is carried out singeing;

[0059] B. Immerse the hemp fiber after singeing in alkaline solution to remove surface impurities and residual pulp;

[0060] C, the hemp fiber after the alkali treatment is put into clear water and repeatedly rinses and puts into the low-temperature drying box to dry;

[0061] D, the hemp fiber after the dry treatment is immersed in the buffer solution containing phenolic monomer and laccase to carry out biological staining;

[0062] E, the hemp fiber after biological dyeing is carried out color fixation, steam processing;

[0063] F, carry out soaping and washing with the hemp fiber at last.

[0064] In this embodiment, the singeing treatment method in step A is: use a heat shield to press the hemp fiber, and then slide back and forth on the heated metal surface for 3-5 seconds.

[0065] In th...

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PUM

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Abstract

The invention discloses a fibrilia biological dyeing technology based on laccase catalytic polymerization reaction. The fibrilia biological dyeing technology comprises the following steps: A, carryingout singeing treatment on fibrilia; B, immersing and treating singed fibrilia into an alkaline solution, and removing surface impurities and residual slurry; C, putting and repeatedly washing the fibrilia after alkaline treatment in clear water, and putting and drying the fibrilia in a low-temperature drying oven; D, immersing the fibrilia after the drying treatment in a buffer solution containing a phenols monomer and laccase, and carrying out biological dyeing; E, carrying out color fixing and steaming treatment on the fibrilia after the biological dyeing; F, finally carrying out soap boiling and water washing on the fibrilia. The fibrilia biological dyeing technology adopted by the invention is simple in operation and low in cost, is environment-friendly and pollution-free and is capable of improving dyeing and color fixing effects of the fibrilia.

Description

technical field [0001] The invention relates to the technical field of hemp fiber dyeing, in particular to a biological dyeing process of hemp fiber based on laccase-catalyzed polymerization reaction. Background technique [0002] In recent years, with the increasingly stringent environmental protection regulations at home and abroad, the clean dyeing and processing of various fibers has received high attention. Traditional dyeing methods and theories based on small molecule synthetic dyes face many challenges, mainly reflected in: complex preparation process of synthetic dyes, large environmental pollution; high requirements for dyeing conditions (often requiring harsh pH value and high temperature), complex dyeing process, and water consumption. High energy consumption and difficult treatment of dyeing wastewater. Commonly used dyes have low molecular weight, dyed products have poor rubbing fastness, low tinting strength, low dye utilization rate, light fastness and heat ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D06P1/44D06P3/60D06P5/02D06L1/06D06L1/12
CPCD06L1/06D06L1/12D06P1/445D06P3/60D06P5/02
Inventor 韩甜甜
Owner 南通霆川电子科技有限公司
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