Preparation method of high-damping and high-strength polyurethane foam
A polyurethane foam and high-strength technology, applied in the field of foam manufacturing, can solve the problems of poor anti-seismic effect, low damping coefficient, and low mechanical strength, and achieve the effect of enhancing thermal insulation effect, high damping coefficient, and improving mechanical properties
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Embodiment 1
[0038] A kind of preparation method of high damping high strength polyurethane foam, described preparation method comprises the following steps:
[0039] (1) Preparation of filler:
[0040] (a) Precursor preparation: add 10 parts of magnesium chloride, 10 parts of boric acid, 5 parts of water and 0.5 parts of polyvinylpyrrolidone into the reaction kettle according to the parts by weight and stir to form a slurry, then add titanium tetrachloride dropwise 3 parts, stirred and reacted at 45°C for 1 to 5 hours, and dried into a block precursor after the stirred reaction;
[0041] (b) High-temperature sintering: Add 1 part of potassium chloride to the precursor obtained in step (a), and then raise the temperature to 650°C. After 4 hours of high-temperature solid-state reaction, gradually increase the temperature at a rate of 2°C / min. High temperature to 900°C, heat preservation for 3 hours to obtain boron titanium magnesium crystal block;
[0042] (c) Separation: Under the action...
Embodiment 2
[0049] A kind of preparation method of high damping high strength polyurethane foam, described preparation method comprises the following steps:
[0050] (1) Preparation of filler:
[0051] (a) Precursor preparation: Add 10 parts of magnesium chloride, 12 parts of boric acid, 5 parts of water and 1 part of polyvinylpyrrolidone into the reaction kettle according to parts by weight and stir to form a slurry, then add titanium tetrachloride dropwise 5 parts, stirred and reacted at 75°C for 2 hours, and dried into a block precursor after the stirred reaction;
[0052] (b) High-temperature sintering: Add 2 parts of potassium chloride to the precursor obtained in step (a), and then raise the temperature to 650°C. After 5 hours of high-temperature solid-state reaction, gradually increase the temperature at a rate of 3°C / min High temperature to 900°C, heat preservation for 4 hours to obtain boron titanium magnesium crystal block;
[0053] (c) Separation: Under the action of ultrasou...
Embodiment 3
[0060] A kind of preparation method of high damping high strength polyurethane foam, described preparation method comprises the following steps:
[0061] (1) Preparation of filler:
[0062] (a) Precursor preparation: add 10 parts of magnesium chloride, 15 parts of boric acid, 5 parts of water and 1.5 parts of polyvinylpyrrolidone into the reaction kettle according to parts by weight and stir to form a slurry, then add titanium tetrachloride dropwise 5 parts, stirred and reacted at 70°C for 3 hours, and dried into a block precursor after the stirred reaction;
[0063] (b) High-temperature sintering: Add 3 parts of potassium chloride to the precursor obtained in step (a), and then raise the temperature to 650°C. After 6 hours of high-temperature solid-state reaction, gradually increase the temperature at a rate of 4°C / min High temperature to 900°C, heat preservation for 4 hours to obtain boron titanium magnesium crystal block;
[0064] (c) Separation: The boron, titanium and m...
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