Etching station aluminum anode oxidation component regeneration preparation technology

A technology of anodizing and preparation process, applied in the direction of anodizing, metal material coating process, superimposed layer plating, etc., can solve the problems of increased maintenance cost, increased component loss, poor adsorption capacity, etc., to increase the number of repeated regenerations , Avoid loss and deformation, reduce the effect of the operation process

Inactive Publication Date: 2019-01-08
芜湖通潮精密机械股份有限公司
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  • Abstract
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  • Claims
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Problems solved by technology

[0004] In the process of using the above method to prepare components, since the plasma spraying uses powder with a particle size of 10-90 μm, the adsorption capacity of spraying on the anodized film is poor, and it needs to be sprayed on the anodized film. Before anodizing, sandblasting is performed on the working surface of the component to improve the adhesion of the coating. Sandblasting increases the loss of the component and causes deformation of the component. With the increase in the number of regenerations of the component, the thickness of the component is seriously reduced and the flatness becomes larger due to deformation. , unable to meet the requirements of use, had to be replaced with new parts, increasing maintenance costs
In addition, the surface roughness of the yttrium oxide coating prepared by plasma spraying is Ra4-8μm, and the porosity of the coating is 3-8%. With the development of the semiconductor and liquid crystal panel industries, the plasma etching atmosphere in the high-process etching chamber is even harsher. , the etching power is getting higher and higher, and the corrosion resistance of ordinary plasma sprayed yttrium oxide coatings is increasingly unable to meet the requirements

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  • Etching station aluminum anode oxidation component regeneration preparation technology
  • Etching station aluminum anode oxidation component regeneration preparation technology

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Embodiment Construction

[0030] The process for preparing the regeneration of the aluminum parts of the etching machine of the present invention comprises the following steps

[0031] Step 1: Degreasing: Degreasing the aluminum parts, the concentration of the degreasing agent is 30-60g / L, the temperature is 40-60°C, and the degreasing time is 4-8min;

[0032] Step 2: Alkali etching: put the degreased aluminum parts into NaOH solution for alkali etching, the concentration of alkali solution is 40-80g / L, the temperature is 40-60°C, and the alkali etching time is 10-20S;

[0033] Step 3: Deashing: put the parts after alkali etching into HNO3 solution to remove ash, the concentration of HNO3 is 30wt% ~ 50wt%, and the ash removal time is 30 ~ 50S;

[0034] Step 4: Washing: Rinse the surface of the component with deionized water for 3 to 5 times, each time for 30 to 50 seconds;

[0035] Step 5: Anodizing: use mixed acid of oxalic acid and sulfuric acid or oxalic acid to anodize aluminum parts, the acid con...

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Abstract

The invention discloses an etching station aluminum anode oxidation component regeneration preparation technology. The etching station aluminum anode oxidation component regeneration preparation technology comprises the following steps: step one, carrying out ungrease treatment on an aluminum component; step two, putting the aluminum component into an alkaline liquor for alkali corrosion; step three, putting the aluminum component into an acid liquor for ash removal; step four, washing; step five, carrying out anode oxidation on the aluminum component; step six, cleaning and drying; step seven, using a tri-cathode plasma spray gun to spray a sizing agent onto an anode oxidation layer of the aluminum component, uniformly controlling the thickness of a sprayed coating to be 60 to 150 microns; step eight, drying and cleaning; and step nine, drying, cooling and packaging. Compared with the prior art, sand blasting pretreatment does not need to be carried out on the component, the anode oxidation layer also does not need sealing treatment, the operation procedure is reduced, the cost is reduced, the productivity is improved, simultaneously, the loss and deformation caused by a sand blasting technology for the component are avoided, and the number of times of repeated regeneration for the component is increased.

Description

technical field [0001] The present invention relates to etching processes. Background technique [0002] The etching process is one of the key processes in the process of semiconductor and liquid crystal panel preparation. The etching machine components are in an active plasma atmosphere when they are working, such as halogen plasma etching gases SF6, CF4, Cl2, etc., which are physically impacted by ions for a long time and chemical etching of active atoms. There are many aluminum parts inside the etching machine, and the cleanliness inside the etching machine is strictly required during the preparation of semiconductors and liquid crystal panels, which requires improving the corrosion resistance of the aluminum parts inside the etching chamber. [0003] The existing technology is to prepare an anodized layer on the surface of aluminum parts, and then use traditional plasma spraying to prepare yttrium oxide coating on the anodized layer. Yttrium oxide has excellent corrosio...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C23C4/11C23C4/134C23C28/04C25D11/08C25D11/10C25D11/16
CPCC23C28/04C25D11/08C25D11/10C25D11/16C23C4/11C23C4/134
Inventor 何新玉司奇峰赵浩
Owner 芜湖通潮精密机械股份有限公司
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