Composite material with high energy storage density and charge-discharge performance, and preparation method of composite material
A technology with charge-discharge performance and high energy storage density, which is applied to components, circuits, capacitors, etc. of fixed capacitors. It can solve the problems of low energy storage density and achieve the effect of good temperature stability and superior charge and discharge performance
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Embodiment 1
[0030] (1) select the raw material Bi whose purity is greater than 99% 2 o 3 , Na 2 CO 3 , SrCO 3 ,TiO 2 and MgO as raw materials for 0-3 type composites. According to chemical formula (Bi 0.32 Sr 0.42 Na 0.2 □ 0.06 )TiO 3 Weigh the material, add absolute ethanol and zirconia balls into the nylon tank for ball milling, discharge, and dry. The ball milling time was 8 hours, and the drying temperature was 120°C. Put the dried powder into a corundum crucible, cover the crucible after compaction, put it into a muffle furnace for calcination, raise it to 850°C at 5°C / min, keep it warm for 2 hours, cool it down to room temperature, and take it out with a grinder. Grinding in a bowl, pouring it into a corundum crucible again for compaction and calcining, the heating rate and holding time are the same as the first time.
[0031] (2) Adding the MgO raw material with a mass fraction of 3wt% to the powder obtained in step (1), and performing secondary ball milling, dischargin...
Embodiment 2
[0038] (1) select the raw material Bi whose purity is greater than 99% 2 o 3 , Na 2 CO 3 , SrCO 3 ,TiO 2 and MgO as raw materials for 0-3 type composites. According to chemical formula (Bi 0.32 Sr 0.42 Na 0.2 □ 0.06 )TiO 3 Weigh the material, add absolute ethanol and zirconia balls into the nylon tank for ball milling, discharge, and dry. The ball milling time was 8 hours, and the drying temperature was 120°C. Put the dried powder into a corundum crucible, cover the crucible after compaction, put it into a muffle furnace for calcination, raise it to 850°C at 5°C / min, keep it warm for 2 hours, cool it down to room temperature, and take it out with a grinder. Grinding in a bowl, pouring it into a corundum crucible again for compaction and calcining, the heating rate and holding time are the same as the first time.
[0039] (2) Adding the MgO raw material with a mass fraction of 3wt% to the powder obtained in step (1), and performing secondary ball milling, dischargin...
Embodiment 3
[0045] (1) select the raw material Bi whose purity is greater than 99% 2 o 3 , Na 2 CO 3 , SrCO 3 ,TiO 2 and MgO as raw materials for 0-3 type composites. According to chemical formula (Bi 0.32 Sr 0.42 Na 0.2 □ 0.06 )TiO 3 Weigh the material, add absolute ethanol and zirconia balls into the nylon tank for ball milling, discharge, and dry. The ball milling time was 8 hours, and the drying temperature was 120°C. Put the dried powder into a corundum crucible, cover the crucible after compaction, put it into a muffle furnace for calcination, raise it to 850°C at 5°C / min, keep it warm for 2 hours, cool it down to room temperature, and take it out with a grinder. Grinding in a bowl, pouring it into a corundum crucible again for compaction and calcining, the heating rate and holding time are the same as the first time.
[0046] (2) Adding the MgO raw material with a mass fraction of 3wt% to the powder obtained in step (1), and performing secondary ball milling, dischargin...
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