A high-throughput preparation method of magnesium alloy bulk materials based on powder jet smelting
A high-throughput technology for magnesium alloys, applied in the field of high-throughput experiments of materials, can solve the problems of long cycle time, long time consumption, burning loss and other problems of magnesium alloys, and achieve the effect of safety in the smelting process
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Embodiment 1
[0030] Thirty Mg-(3.8~3.3)Zn-(0.3~0.7)Gd at% magnesium alloy samples with different compositions were smelted at the same melting temperature. First select the equipment. A multi-component real-time control precision powder feeding system (based on the patent 201610323445.2 self-installed powder feeding system), a five-temperature zone tubular atmosphere furnace (OTF-1200X-V, a furnace tube diameter of 50mm and a length of 1400mm, and a stable heating zone length of 180mm, A total of 5 heating zones), vacuum glove box and other commercial equipment, and customize the turntable crucible bracket and crucible size according to the commercial equipment. Among them, the size of the crucible is: the outer radius of the cylinder is 10mm, the inner radius is 5m, the height is 25mm, and the bottom thickness is 5mm; the semicircle diameter of the ears is 6mm, the length of the ears is 5mm, one ear is 0mm from the crucible mouth, and the other ear is 5mm from the crucible mouth , each c...
Embodiment 2
[0037] Mg-3.5Zn-0.6Gd at% magnesium alloy samples with the same composition were melted at five melting temperatures. The equipment selection conditions refer to Example 1, followed by high-throughput preparation of magnesium alloy bulk materials based on powder jet smelting. According to the instructions, the four steps of multi-component real-time precision output of alloy powder, continuous feeding of crucible, packaging of crucible, and partition melting of alloy powder in multi-temperature zones are carried out sequentially. The first three steps need to be carried out in a vacuum glove box. within.
[0038] 100-mesh Zn powder, Gd powder, and Mg powder are respectively loaded into the powder supply cylinder of the multi-component powder feeding system; the air inlet pressure of each powder supply hopper and the powder wheel, and the speed of the powder wheel are adjusted so that the total powder feeding rate is 20g / min, and the powder composition sent out is Mg-3.5Zn-0....
Embodiment 3
[0043] Thirty samples of Mg-(3.8~3.3)Zn-(0.3~0.7)Gd at% magnesium alloys with different compositions were melted at five melting temperatures. The equipment selection conditions refer to Example 1, followed by high-throughput preparation of magnesium alloy bulk materials based on powder jet smelting. According to the instructions, the four steps of multi-component real-time precision output of alloy powder, continuous feeding of crucible, packaging of crucible, and partition melting of alloy powder in multi-temperature zones are carried out sequentially. The first three steps need to be carried out in a vacuum glove box. within.
[0044] The configuration of 30 magnesium alloy samples with different compositions Mg-(3.8-3.3)Zn-(0.3-0.7)Gd at% was completed in the manner described in Example 1.
[0045] Loosen the fastening bolts on the crucible chain. The 6 magnesium alloy samples whose composition is Mg-(3.8~3.3)Zn-0.3Gd at% are the first group, cover the crucible cover, sc...
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