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Calcium sulfate whisker aerogel foam concrete and preparation method thereof

A calcium sulfate whisker and foam concrete technology, which is applied in the fields of civil construction and thermal insulation materials, can solve the problems of reduced mechanical properties of foam concrete, difficulty in obtaining ultra-light foam concrete, and affecting the engineering application of foam concrete, so as to improve the blockability, Good high temperature resistance, strong flexibility effect

Active Publication Date: 2019-03-01
GUANGZHOU UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Patent CN 205804646 U proposes an airgel foam concrete insulation and fireproof board, which has low density, low thermal conductivity, and low water absorption, but the interface strength between airgel and cementitious materials is often low, resulting in foam concrete The mechanical properties are significantly reduced, and it is easy to cause the airgel powder to fall off from the concrete matrix, which seriously affects the engineering application of foam concrete
In the literature "Preparation and Performance Experimental Research of Lightweight Low Thermal Conductivity Airgel Foam Concrete", a density of 270.2kg / m 3 , Ultra-light foam concrete with a thermal conductivity of 0.069W / (m.K), but the foam concrete produced has disadvantages such as uneven pore size and low strength, and it is difficult to obtain ultra-light foam concrete with high mechanical properties

Method used

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  • Calcium sulfate whisker aerogel foam concrete and preparation method thereof

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Embodiment 1

[0037]The present embodiment prepares calcium sulfate whisker clay airgel foam concrete, is to take clay airgel powder as filling material, and its particle diameter is 85 orders (about 162 μ m), porosity is 95%, and pore diameter is 45nm; Dispersed calcium sulfate whiskers are reinforcements with a diameter of 1 μm and an aspect ratio of 10. Concrete preparation steps are as follows:

[0038] (1) Mix water and organic bentonite according to the mass ratio of 1000:1.5, and stir evenly to obtain thickened water;

[0039] (2) Carry out dry mixing with silicate PO42.5 cement and clay airgel powder, then add the thickening water that step (1) obtains, stir well, obtain clay airgel concrete slurry; Wherein silicate The mass ratio between PO42.5 cement, clay airgel powder and thickening water is 1:0.10:0.7;

[0040] (3) Slowly add dispersed calcium sulfate whiskers into the clay airgel concrete slurry obtained in step (2), stir evenly to obtain calcium sulfate whiskers / clay airgel...

Embodiment 2

[0044] The present embodiment prepares calcium sulfate whisker carbon airgel foam concrete, is to take carbon airgel powder as filling material, and its particle diameter is 80 orders (about 180 μ m), porosity is 93%, and pore diameter is 40nm; Dispersed calcium sulfate whiskers are reinforcements with a diameter of 5 μm and an aspect ratio of 100. Concrete preparation steps are as follows:

[0045] (1) Mix water and barstone soil in a mass ratio of 1000:3, and stir evenly to obtain thickened water;

[0046] (2) Carry out dry mixing with magnesium oxychloride PO42.5 cement and carbon airgel powder, then add the thickening water prepared in step (1), stir evenly, obtain carbon airgel concrete slurry; The mass ratio between magnesium PO 42.5 cement, carbon airgel powder and thickening water is 1:0.2:0.8;

[0047] (3) Slowly add calcium sulfate whiskers in dispersed form into the carbon airgel concrete slurry obtained in step (2), stir evenly to obtain calcium sulfate whisker / c...

Embodiment 3

[0051] The present embodiment prepares calcium sulfate whisker SiO 2 Airgel foam concrete, based on SiO 2 Airgel powder is used as filling material, its particle size is 70 mesh (about 212μm), porosity is 90%, and pore diameter is 35nm; dispersed calcium sulfate whiskers are used as reinforcement, diameter is 10μm, aspect ratio for 500. Concrete preparation steps are as follows:

[0052] (1) Mix water and diatomaceous earth in a mass ratio of 1000:5, and stir evenly to obtain thickened water;

[0053] (2) Combine sulfoaluminate PO 42.5 cement with SiO 2 The airgel powder is dry-mixed, and then the thickened water prepared in step (1) is added, and stirred evenly to obtain SiO 2 Airgel concrete paste; the sulphoaluminate PO 42.5 cement, SiO 2 The mass ratio between airgel powder and thickening water is 1:0.3:0.9;

[0054] (3) Slowly add dispersed calcium sulfate whiskers to the SiO obtained in step (2) 2 In the airgel concrete slurry, stir evenly to get calcium sulfate w...

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Abstract

The invention discloses calcium sulfate whisker aerogel foam concrete and a preparation method thereof. The calcium sulfate whisker aerogel foam concrete comprises cementing materials, aerogel powder,calcium sulfate whiskers, thickening agents, foaming agents and water, the weight ratio of the cementing materials, the aerogel powder to the calcium sulfate whiskers is 1:(0.01-0.3):(0.001-0.01), the diameter of the calcium sulfate whiskers is 1-10 micrometers, the long-diameter ratio of the calcium sulfate whiskers is 10-500, low-cost calcium sulfate whiskers are mixed into an aerogel foam concrete substrates, calcium sulfate whiskers with high long-diameter ratio have high flexibility and are high in bonding efficiency, so that expansion of cracks of the aerogel foam concrete substrates can be decreased, mechanical property and block forming property of the aerogel foam concrete are remarkably improved, and a preparation process is simplified, and the concrete can be widely applied tothe field of heat insulation of building walls, filling of roads, sound insulation of barriers and the like.

Description

technical field [0001] The invention belongs to the field of civil construction and thermal insulation materials, and in particular relates to a calcium sulfate whisker airgel foam concrete and a preparation method thereof. Background technique [0002] Foam concrete is an energy-saving and environment-friendly wall insulation material. It has the characteristics of low density, good thermal insulation, strong sound insulation and fire resistance, and excellent earthquake resistance. It is widely used in building energy conservation and other fields. However, lightweight foam concrete also has certain limitations, such as low strength, water absorption and cracking. [0003] With the rapid development of foam concrete, new types of foam concrete mixed with various external materials have appeared on the market, and airgel foam concrete is the lightest foam concrete; airgel is a lightweight porous, Amorphous solid material with super thermal insulation performance, the incor...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C04B28/04C04B28/32C04B28/06C04B28/08C04B28/02C04B28/10C04B28/14C04B28/26C04B26/26C04B26/02C04B38/10C04B38/08C04B111/28
CPCC04B26/02C04B26/26C04B28/021C04B28/04C04B28/06C04B28/08C04B28/10C04B28/14C04B28/26C04B28/32C04B38/106C04B2111/285C04B14/104C04B22/002C04B14/10C04B14/383C04B24/34C04B38/08C04B38/0067C04B14/028C04B14/102C04B2103/42C04B14/064C04B14/08C04B24/10
Inventor 吴会军付平杨丽修徐涛
Owner GUANGZHOU UNIVERSITY
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