A water-based drilling fluid for protecting oil and gas reservoirs with high temperature and calcium resistance and its application
A technology for water-based drilling fluids and oil and gas reservoirs, applied in the field of water-based drilling fluids, can solve the problems of large consumption of treatment agents, scrapped wellbore, polluted reservoirs, etc.
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preparation example Construction
[0026] In the water-based drilling fluid of the present invention, the preparation method of the above-mentioned fluid loss control agent comprises: in the presence of sodium lauryl sulfate and 2,2-azobis(2-methylpropylimidium) dihydrochloride, The monomer M1 shown in formula (4), the monomer M2 shown in formula (5), and the monomer M3 shown in formula (6) are polymerized in water as a solvent,
[0027]
[0028] Among them, R 1 , R 2 , R 3 , R 4 , R 5 , R 6 , R 7 , R 9 , R 10 and R 11 each independently hydrogen, C 1 -C 4 Alkyl or C 1 -C 4 Alkoxy, preferably hydrogen, methyl, ethyl, methoxy or ethoxy; R 8 from C 1-C 4 The alkylene group is preferably methylene or ethylene.
[0029] In the above preparation method of fluid loss control agent, the mass ratio of the monomer M1, the monomer M2 and the monomer M3 is (0.1-0.2):1:(0.05-0.1), preferably (0.1 -0.15):1:(0.05-0.075), more preferably (0.12-0.15):1:(0.055-0.07).
[0030] In the above-mentioned preparat...
preparation example 1
[0066] Adjust the temperature of the water bath to 80°C, dissolve sodium lauryl sulfate in distilled water and pour it into a three-neck flask, stir with a magnetic force at an appropriate speed for 15 minutes; add 100g of distilled water to a 100ml beaker, and add formula (4-1) The monomer M1 shown, the monomer M2 shown in the formula (5-1), and the monomer M3 shown in the formula (6-1). After it is completely dissolved, add it to the three-necked flask, and stir for 30 minutes under the protection of nitrogen; dissolve 2,2-azobis(2-methylpropylimidium) dihydrochloride in distilled water, and then add it dropwise to the three-necked flask Among them, the mass ratio of monomers M1, M2 and M3 is 0.15:1:0.075, monomer M2, sodium lauryl sulfate and 2,2-azobis(2-methylpropylimidium) dihydrochloride The mass ratio is 200:0.5:0.4. After reacting for 5 hours, copolymer A1 was obtained with a number average molecular weight of 42,000.
[0067]
preparation example 2
[0069] Adjust the temperature of the water bath to 80°C, dissolve sodium lauryl sulfate in distilled water and pour it into a three-neck flask, stir with a magnetic force at an appropriate speed for 15 minutes; add 100g of distilled water to a 100ml beaker, and add formula (4-2) The monomer M1 shown, the monomer M2 shown in the formula (5-1), and the monomer M3 shown in the formula (6-1). After it is completely dissolved, add it to the three-necked flask, and stir for 30 minutes under the protection of nitrogen; dissolve 2,2-azobis(2-methylpropylimidium) dihydrochloride in distilled water, and then add it dropwise to the three-necked flask Among them, the mass ratio of monomers M1, M2 and M3 is 0.1:1:0.05, monomer M2, sodium lauryl sulfate and 2,2-azobis(2-methylpropylimidium) dihydrochloride The mass ratio is 100:0.3:0.2. Copolymer A2 was obtained after reacting for 5 hours, and its number average molecular weight was 20,000.
[0070]
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