Self-repairing aramid fiber reinforced core for optical cable, and preparation method of self-repairing aramid fiber reinforced core
An aramid fiber strengthening and self-repairing technology, which is applied in the field of optical cables and optical cable materials, can solve the problems of low interlayer shear strength, high degree of orientation of molecular chains on the surface, and material damage, so as to improve mechanical properties and service life, enhance Self-healing performance, the effect of enhancing overall performance
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Embodiment 1
[0029] A self-repairing aramid fiber reinforced core for optical cable, comprising an aramid fiber substrate, a polydopamine layer on the surface of the aramid fiber substrate, and a polyurethane layer coated on the surface of the polydopamine layer; the polyurethane layer is doped with boron nitride nanosheets ; The content of boron nitride nanosheets in the polyurethane layer is 5wt%; the thickness of the polyurethane layer is 0.5mm;
[0030] The polyurethane in the polyurethane layer is self-healing polyurethane, and the preparation process of self-healing polyurethane includes:
[0031] S1. Mix diphenylmethane diisocyanate and poly-1,4-butylene adipate diol in a molar ratio of 1.8:1, add DMF to dissolve, heat up to 70°C for 3 hours in a nitrogen atmosphere, and cool down to 0°C; add furfurylamine dropwise to react for 2 hours, raise the temperature to 30°C, continue to react for 4 hours, precipitate and filter to obtain a furan-terminated intermediate; wherein, the molar v...
Embodiment 2
[0038] A self-repairing aramid fiber reinforced core for optical cable, comprising an aramid fiber substrate, a polydopamine layer on the surface of the aramid fiber substrate, and a polyurethane layer coated on the surface of the polydopamine layer; the polyurethane layer is doped with boron nitride nanosheets ; The content of boron nitride nanosheets in the polyurethane layer is 15wt%; the thickness of the polyurethane layer is 3mm;
[0039] The polyurethane in the polyurethane layer is self-healing polyurethane, and the preparation process of self-healing polyurethane includes:
[0040] S1. Mix diphenylmethane diisocyanate and poly-1,4-butylene adipate diol in a molar ratio of 2.2:1, add DMF to dissolve, heat up to 80°C for 2 hours in a nitrogen atmosphere, and cool down to 5°C; add furfurylamine dropwise for 1 hour, raise the temperature to 40°C, continue the reaction for 3 hours, precipitate and filter to obtain a furan-terminated intermediate; wherein, the molar volume r...
Embodiment 3
[0047] A self-repairing aramid fiber reinforced core for optical cable, comprising an aramid fiber substrate, a polydopamine layer on the surface of the aramid fiber substrate, and a polyurethane layer coated on the surface of the polydopamine layer; the polyurethane layer is doped with boron nitride nanosheets ; The content of boron nitride nanosheets in the polyurethane layer is 10wt%; the thickness of the polyurethane layer is 2mm;
[0048] The polyurethane in the polyurethane layer is self-healing polyurethane, and the preparation process of self-healing polyurethane includes:
[0049] S1. Mix diphenylmethane diisocyanate and poly-1,4-butylene adipate diol in a molar ratio of 2:1, add DMF to dissolve, heat up to 75°C in a nitrogen atmosphere and react for 2.5h, then cool down to 3°C; add furfurylamine dropwise to react for 1.5h, raise the temperature to 35°C, continue to react for 3.5h, precipitate and filter to obtain a furan-terminated intermediate; wherein, the molar vo...
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