Method of producing high fructose corn syrup and glucose in same production line

A fructose syrup and production method technology, applied in the same-line production process of glucose, in the field of fructose syrup, can solve the problems of high production cost and difficulty in industrial production, reduce steam consumption, reduce the risk of continuity, and realize energy saving The effect of emission reduction

Inactive Publication Date: 2019-03-29
河南飞天生物科技股份有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The industrial production of fructose syrup and glucose is currently mainly obtained from starch as raw material through liquid saccharification and refining. Due to the diffe

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0032] The production process of glucose syrup is as follows:

[0033] (I) Sizing: Sizing starch and water to 23 degrees Baume to obtain a mixed starch slurry;

[0034] (II) Liquefaction: adjust the pH of the mixed starch slurry in step (I) to 5.6, add high temperature resistant α-amylase 0.3Kg / ton dry basis, the first injection temperature is 105°C, and liquefy in laminar flow after flash evaporation The tank is kept warm for 90 minutes; the temperature of the second injection is 125°C;

[0035] (Ⅲ) Saccharification: After liquefaction, add sweet water or pure water, adjust the concentration of the liquefied liquid to 32%, adjust the pH to 4.2, add glucoamylase to the liquefied liquid at a dry basis of 0.3Kg / ton, and keep warm at 60°C for 60 hours , to obtain glucose saccharification liquid, the DX value of the saccharification liquid is ≥96%;

[0036] (Ⅳ) Deslagging filtration, pre-concentration, decolorization: add the saccharification liquid obtained in step (Ⅲ) to diato...

Embodiment 2

[0048] The production process of glucose syrup is as follows:

[0049] (I) Sizing: Sizing starch and water to 24 degrees Baume to obtain a mixed starch slurry;

[0050] (II) Liquefaction: adjust the pH of the mixed starch slurry in step (I) to 5.8, add high temperature resistant α-amylase 0.4Kg / ton dry basis, the first injection temperature is 108°C, and liquefy in laminar flow after flash evaporation The tank is kept warm for 100 minutes; the temperature of the second injection is 128°C;

[0051] (Ⅲ) Saccharification: After liquefaction, add detached sweet water or pure water, adjust the concentration of the liquefied liquid to 32.5%, adjust the pH to 4.3, add glucoamylase to the liquefied liquid at a dry basis of 0.4Kg / ton, and incubate at 61°C for 50 hours , to obtain glucose saccharification liquid, the DX value of the saccharification liquid is ≥96%;

[0052] (Ⅳ) Deslagging filtration, pre-concentration, decolorization: add the saccharification liquid obtained in step (...

Embodiment 3

[0064] The production process of glucose syrup is as follows:

[0065] (I) Sizing: Sizing starch and water to 25 degrees Baume to obtain a mixed starch slurry;

[0066] (II) Liquefaction: adjust the pH of the mixed starch slurry in step (I) to 6.0, add high temperature resistant α-amylase 0.5Kg / ton dry basis, the first spraying temperature is 109°C, and liquefy in laminar flow after flash evaporation The tank is kept warm for 120 minutes; the temperature of the second injection is 130°C;

[0067] (Ⅲ) Saccharification: After liquefaction, add sweet water or pure water, adjust the concentration of the liquefied liquid to 33%, adjust the pH to 4.4, add glucoamylase to the liquefied liquid at a dry basis of 0.5Kg / ton, and incubate at 62°C for 48 hours , to obtain glucose saccharification liquid, the DX value of the saccharification liquid is ≥96%;

[0068] (Ⅳ) Deslagging filtration, pre-concentration, decolorization: add the saccharification solution obtained in step (Ⅲ) to diat...

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Abstract

The invention provides a method of producing high fructose corn syrup and glucose in a same production line. A certain amount of glucose syrup is added into a mother liquor so that the mixture can meet the requirements of monosaccharide components of F42 high fructose corn syrup; the mixture is subjected to isomerization so as to convert glucose into fructose after isomerization; and then discoloring, ion exchanging, concentrating, and packaging are performed to produce F42 fructose syrup. A conventional glucose production technology is optimized, a high concentration liquefying production method is adopted; high fructose corn syrup and glucose are co-produced; the byproducts of glucose are recovered and reutilized; investment, water resources, and energy are saved, and energy saving and emission reduction are realized.

Description

technical field [0001] The invention relates to the field of syrup preparation, in particular to a simultaneous production process of fructose syrup and glucose. Background technique [0002] Fructose syrup is mainly composed of glucose and fructose. According to the fructose content, fructose syrup is divided into three categories: the first generation fructose syrup (F42 type) contains 42% fructose; the second generation fructose syrup (F55 type) contains 55% fructose; the third generation fructose syrup (F90 type) type) containing 90% fructose. The sweetness of fructose syrup is positively correlated with the fructose content, and the third-generation fructose syrup can be used in a small amount in food to achieve a certain sweetness. Since the sweetness of fructose syrup is comparable to that of sucrose and has its own characteristics, its application field is wider than that of sucrose; it is not only widely used in food industry and health food, but also in pharmaceu...

Claims

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Application Information

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IPC IPC(8): A23L29/30C07H1/06C07H3/02
CPCA23V2002/00A23L29/30C07H1/06C07H3/02A23V2250/61A23V2250/606
Inventor 李林海董得平赵桂强高素珍魏利军
Owner 河南飞天生物科技股份有限公司
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