Far-infrared functional master batch, far-infrared polyester fiber as well as preparation method and application

A technology of functional masterbatch and polyester fiber, which is applied in the field of far-infrared polyester fiber and its preparation, and far-infrared functional masterbatch, which can solve the problems of poor durability and water resistance, low far-infrared radiation, and poor matching of resonance bands. To achieve the effect of improving the efficacy of far infrared

Inactive Publication Date: 2019-03-29
岑锴林
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  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0009] The current far-infrared fiber is mainly prepared by post-processing and finishing technology, and the active ingredient with far-infrared effect is formed on the fiber in the form of surface wrapping. The content of the active ingredient is very limited, resulting in low far-infrared radiation, which is suitable for water molecule excitation. The problem of poor far-infrared efficacy such as poor resonance band matching of far-infrared radiation; at the same time, the fiber with far-infrared efficacy also has the problems of poor durability and water resistance, and a single PET fiber is prone to static electricity, so it is necessary to provide a A polyester fiber with good far-infrared efficacy, durability and washing resistance, and antistatic effect

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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  • Far-infrared functional master batch, far-infrared polyester fiber as well as preparation method and application
  • Far-infrared functional master batch, far-infrared polyester fiber as well as preparation method and application
  • Far-infrared functional master batch, far-infrared polyester fiber as well as preparation method and application

Examples

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preparation example Construction

[0047] The preparation method of the far-infrared polyester fiber of one embodiment, comprises the following steps S110~S120:

[0048] S110. Provide PET and far-infrared functional masterbatches.

[0049] Among them, the intrinsic viscosity of PET is 0.62-0.73.

[0050] Concrete, the preparation method of PET is as follows:

[0051] Dimethyl terephthalate and ethylene glycol with a molar ratio of 1:(2~2.3) are polycondensed at high temperature under the action of manganese acetate catalyst.

[0052] It can be understood that the above-mentioned PET can also be prepared by other existing methods or purchased directly, as long as the intrinsic viscosity is 0.62-0.73.

[0053] Specifically, the far-infrared functional masterbatch is prepared by the following steps S1101-S1105:

[0054] S1101. Provide silver-loaded titanium dioxide / graphene nanoparticles (Ag@TiO 2 / GO).

[0055] Wherein, the silver-loaded titanium dioxide / graphene nanoparticles are prepared by the following s...

Embodiment 1

[0077] (1) Synthesis of PET fibers: Dimethyl terephthalate and ethylene glycol with a molar ratio of 1:2.2 are produced by high-temperature polycondensation under the action of catalyst manganese acetate, and the intrinsic viscosity is 0.68.

[0078] (2) Synthesis of PETG fiber: Dimethyl terephthalate, ethylene glycol and 1,4-cyclohexanedimethanol with a molar ratio of 1:1.8:0.3 are made by high-temperature polycondensation under the action of a catalyst. Viscosity number 0.65.

[0079] (3) Preparation of silver-loaded titanium dioxide / graphene (Ag@TiO2 / GO) particles: add an appropriate amount of polyvinylpyrrolidone (PVP-10) to a certain amount of ethylene glycol, stir to dissolve completely, and then add metered AgN03 , forming a clear and transparent solution, and while stirring, the solution was slowly heated to 120°C and kept for 1h. After the solution was cooled, it was extracted with acetone and centrifuged (5000 rpm) to remove the supernatant. The residue was then ce...

Embodiment 2

[0084] Example 2 is basically the same as Example 1, except that the far-infrared functional masterbatch in step (6) in Example 2 is 3 parts.

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Abstract

The invention relates to a far-infrared functional master batch, a far-infrared polyester fiber as well as a preparation method and application. The far-infrared polyester fiber comprises 100 parts byweight of PET (Polyethylene Terephthalate) and 1-5 parts by weight of the far-infrared functional master batches. The far-infrared polyester fiber is capable of sufficiently taking respective advantageous properties of PET and PETG (Polyethylene Terephthalate Glycol) fibers, has excellent bending elasticity resilience and high volume fluffiness, and meanwhile has excellent anion release properties and far-infrared radiation performance, and excellent bacterium prevention and inhibition properties as well.

Description

[0001] This application claims the priority of the Chinese patent application submitted to the China Patent Office on August 14, 2018, with the application number 201810922222.7, and the invention title is "Far-infrared functional masterbatch, far-infrared polyester fiber and its preparation method and application", all of which The contents are incorporated by reference in this application. technical field [0002] The invention relates to the technical field of far-infrared fibers, in particular to a far-infrared functional masterbatch, a far-infrared polyester fiber, a preparation method and an application thereof. Background technique [0003] Polyethylene terephthalate (PET) has the characteristics of high strength, good elasticity, not easy to deform, corrosion resistance, wear resistance, weather resistance, insulation, smooth surface, affordable price, and poor dyeability. my country is the world's largest producer and user of PET, but there are problems such as sing...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): D01F6/92D01F1/10D01F1/09
CPCD01F1/09D01F1/10D01F1/103D01F6/92
Inventor 岑锴林
Owner 岑锴林
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