Sealant for display
A display and encapsulant technology, applied in sealing devices, instruments, adhesives, etc., can solve problems such as display components that have not yet been realized
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Examples
Embodiment 1~10、 comparative example 1~4
[0123] Component (A), component (H ) at 90°C for heating and dissolving, then cooled to room temperature, adding components (C), component (D), component (E), component (F), component (G), component (I), stirred, and then using three Dispersion was performed with a roll machine, and liquid crystal sealing agent Examples 1-10 were prepared by filtering through a metal mesh (635 mesh). In addition, component (A) was removed to prepare comparative examples 1 and 2, and comparative examples 3 and 4 were prepared by using component (A') instead of component (A).
[0124] [Elastic modulus measurement]
[0125] For the liquid crystal sealant produced in Examples and Comparative Examples, the liquid crystal sealant made into a thin film with a thickness of 100 μm sandwiched between polyethylene terephthalate (PET) films was used using a metal halide lamp (USHIO Denki Co., Ltd.) irradiation 3000mJ / cm 2 (100mW / cm2 UV rays for 30 seconds) to cure, and then put into an oven at 120° C. ...
Synthetic example 3
[0148] B-1-4: Partial acrylated product of bisphenol A epoxy resin (synthesis example 4)
[0149] B-1-5: Lactone-modified hydroxypivalic acid neopentyl glycol diacrylate (trade name "KAYARAD HX-620" manufactured by Nippon Kayaku Co., Ltd.)
[0150] B-1-6: Polyester-type urethane acrylate (manufactured by Nippon Kayaku Co., Ltd.; KAYARAD UX-3204)
[0151] B-2-1: Bisphenol A epoxy resin (trade name "RE-310S" manufactured by Nippon Kayaku Co., Ltd.)
[0152] C-1: Pentaerythritol tetrakis (3-mercaptobutyrate) (Showa Denko Co., Ltd. product name "Karenz MT PE1")
[0153] D-1: Polymethacrylate-based organic fine particles (trade name "F-351S" manufactured by Aica Industry Co., Ltd.)
[0154] E-1: Spherical silica (trade name "Sunseal SSP-07M" manufactured by Tokuyama Co., Ltd.)
[0155] F-1: 3-glycidoxypropyltrimethoxysilane (trade name "Sila Ace S-510" manufactured by JNC Corporation)
[0156] F-2: N-2(aminoethyl)-3-aminopropyltriethoxysilane (manufactured by Shin-Etsu Chemical...
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