Flexible red photoelectric injection light-emitting device based on metal halide perovskite light-emitting layer and preparation method thereof
A metal halide, light-emitting device technology, applied in the field of flexible red photoelectric injection light-emitting devices and their preparation, can solve problems such as poor bending stability, achieve good band gap matching, solve the problem of bending stability, and excellent bending resistance. Effect
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[0027] Example 1
[0028] SnO 2 Preparation of sol-gel: weigh 2.79g SnCl 2 ·2H 2 O in 25mL of absolute ethanol, reflux for 3 hours at 78°C, aging at 30°C for 3 hours, and then place it at room temperature for 2 days to obtain a pale yellow sol, which is SnO 2 Sol.
[0029] The method of mixed perovskite precursor fluid: A two-step method was used to prepare a mixed perovskite precursor. A: First, 507.7mg PbI 2 , 80.7mg PbBr 2 , 172mg HC(NH 2 ) 2 I (FAI) and 22mg CH 3 NH 3 Br (MABr), DMF (N, N dimethylformamide) and DMSO (dimethyl sulfoxide) (4:1, volume ratio) are mixed and dissolved in 1 mL of solvent. B: Dissolve 194.9mg CsI in 500uL DMSO. Both solutions were stirred at 60°C for 1 hour, and then precursor B was added to precursor A in a volume ratio of 1:19. The mixed precursor was stirred at 60°C for 1 h.
[0030] Spiro-OMeTAD solution preparation method: weigh the hole transport material Spiro-OMeTAD (CuPc-DMP) 80mg, 20uL Li-TFSI (520mg / 1mL acetonitrile), 30uLTBP, 20uL Co salt...
Example Embodiment
[0031] Example 2:
[0032] This embodiment discloses a flexible red photoelectric injection light-emitting device based on a metal halide perovskite light-emitting layer. The preparation steps are as follows:
[0033] The substrate adopts flexible and bendable PEN / ITO with a layer of ITO on the surface. Using SnO prepared in Example 1 2 Sol-gel, mixed perovskite precursor and Spiro-OMeTAD solution.
[0034] (1) Before preparing the electron transport layer, first use tape to remove 2.5×2.5cm 2 The flexible and bendable PEN / ITO substrate with a layer of ITO on the surface is selectively masked, etched with zinc powder and 2M dilute hydrochloric acid, and then wiped off the remaining zinc powder with cotton. Use detergent, ultrapure water, acetone, and ethanol for ultrasonic cleaning for 30 minutes. After the washed glass is blown dry, treat it with UV-ozone cleaning equipment for 60 minutes, and store it in a dust-free environment for later use.
[0035] (2) Preparation of amorphous ...
Example Embodiment
[0040] Example 3:
[0041] This embodiment discloses a flexible red photoelectric injection light-emitting device based on a metal halide perovskite light-emitting layer. The preparation steps are as follows:
[0042] The substrate adopts flexible and bendable PEN / ITO with a layer of ITO on the surface. Using SnO prepared in Example 1 2 Sol-gel, mixed perovskite precursor and Spiro-OMeTAD solution.
[0043] (1) Before preparing the electron transport layer, first use tape to remove 2.5×2.5cm 2 The flexible and bendable PEN / ITO substrate with a layer of ITO on the surface is selectively masked, etched with zinc powder and 2M dilute hydrochloric acid, and then wiped off the remaining zinc powder with cotton. Use detergent, ultrapure water, acetone, and ethanol for ultrasonic cleaning for 30 minutes. After the washed glass is blown dry, treat it with UV-ozone cleaning equipment for 60 minutes, and store it in a dust-free environment for later use.
[0044] (2) Preparation of amorphous ...
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