Preparation method and application of an aqueous high-voltage electrode material
A high-voltage electrode and water system technology, applied in the field of electrochemical energy storage, can solve the problems of low specific capacitance of the negative electrode, low voltage, high working voltage and high specific capacitance, etc., achieve high capacitance, high voltage window, and increase specific capacitance. Effect
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Embodiment 1
[0037] a) The carbon cloth is ultrasonically cleaned with acetone, ethanol and deionized water in turn.
[0038] b) Prepare 40 mL of 2 mM Co(NO 3 ) 2 ·6H 2 O and 1 mM Zn(NO 3 ) 2 ·6H 2 Solution A of O, 40 mL of solution B containing 20mM 2-methylimidazole, mix A and B under stirring, immerse the carbon cloth obtained in step a) into the mixed solution for 4 hours, take it out and dry it, and then place it in the air at 350°C Calcined for 2 hours under the same conditions to obtain the carbon cloth / carbon nanowall array.
[0039] c) The carbon cloth / carbon nanowall array obtained in step b) was used as a working electrode, and immersed in 50 mL of 0.1 M Mn(CH 3 COO) 2 and 0.1 M Na 2 SO 4 In the electrodeposition solution, the Ag / AgCl electrode was used as the reference electrode, and the platinum sheet electrode was used as the counter electrode. -1 The scanning speed was cycled for 2 cycles, then washed with deionized water, and dried at 60°C. Finally in saturated ...
Embodiment 2
[0043] a) The carbon cloth is ultrasonically cleaned with acetone, ethanol and deionized water in turn.
[0044] b) Prepare 40 mL of 2 mM Co(NO 3 ) 2 ·6H 2 O and 1 mM Zn(NO 3 ) 2 ·6H 2 Solution A of O, 40 mL of solution B containing 20mM 2-methylimidazole, mix A and B under stirring, immerse the carbon cloth obtained in step a) into the mixed solution for 8 hours, take it out and dry it, and then place it in the air at 500°C Calcined for 2 hours under the same conditions to obtain the carbon cloth / carbon nanowall array.
[0045] c) The carbon cloth / carbon nanowall array obtained in step b) was used as a working electrode, immersed in 50 mL of 0.5 M Mn(CH 3 COO) 2 and 0.2 M Na 2 SO 4 In the electrodeposition solution, the Ag / AgCl electrode was used as the reference electrode, and the platinum sheet electrode was used as the counter electrode. -1 The scanning speed was cycled for 5 cycles, then washed with deionized water, and dried at 60°C. Finally in saturated Na ...
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