Laminar composite SiC/graphite film material for thermal management and preparation method thereof
A technology of layered composite material and graphite film, which is applied in the field of SiC/graphite film layered composite material for thermal management and its preparation, can solve problems such as public literature reports of non-SiC ceramic reinforced graphite film layered composite material, and achieve high Strength, ensuring work efficiency and service life, and the effect of simple preparation process
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Embodiment 1
[0026] The first step is the preparation of graphite film coated with SiC ceramic layer:
[0027] 1) According to the molar ratio of Si powder and graphite film as 1:2, take Si powder with a particle size of 5 microns;
[0028] 2) Take NaCl and NaF according to the molar ratio of NaCl and NaF as 1:1, pour them into a mortar, grind them and mix them evenly to obtain mixed salt powder;
[0029] 3) According to the mass ratio of Si powder and mixed salt powder as 1:5, pour Si powder and mixed salt powder into a mortar and grind and mix evenly to obtain coating powder;
[0030] 4) Take the graphite film and coating powder with a thickness of 12 microns and alternately load them layer by layer in the graphite crucible whose inner surface is coated with SiC ceramic layer according to the order of "coating powder-graphite film-coating powder...", cover Put the crucible cover in the heat treatment furnace;
[0031] 5) Vacuumize the heat treatment furnace and feed it with argon gas. ...
Embodiment 2
[0037] The first step is the preparation of graphite film coated with SiC ceramic layer:
[0038] 1) According to the molar ratio of Si powder and graphite film as 2:5, take Si powder with a particle size of 5 microns;
[0039] 2) Take NaCl and NaF according to the molar ratio of NaCl and NaF as 1:1, pour them into a mortar, grind them and mix them evenly to obtain mixed salt powder;
[0040] 3) According to the mass ratio of Si powder and mixed salt powder as 1:5, pour Si powder and mixed salt powder into a mortar and grind and mix evenly to obtain coating powder;
[0041] 4) Take the graphite film and coating powder with a thickness of 50 microns and alternately load them layer by layer in the graphite crucible whose inner surface is coated with SiC ceramic layer according to the order of "coating powder-graphite film-coating powder...", cover Put the crucible cover in the heat treatment furnace;
[0042] 5) Vacuumize the heat treatment furnace and feed it with argon gas. ...
Embodiment 3
[0048] The first step is the preparation of graphite film coated with SiC ceramic layer:
[0049] 1) According to the molar ratio of Si powder and graphite film as 3:10, take Si powder with a particle size of 5 microns;
[0050] 2) Take NaCl and NaF according to the molar ratio of NaCl and NaF as 1:1, pour them into a mortar, grind them and mix them evenly to obtain mixed salt powder;
[0051] 3) According to the mass ratio of Si powder and mixed salt powder as 1:5, pour Si powder and mixed salt powder into a mortar and grind and mix evenly to obtain coating powder;
[0052] 4) Take graphite film and coating powder with a thickness of 40 microns and alternately load them layer by layer into a graphite crucible whose inner surface is coated with a SiC ceramic layer in the order of "coating powder-graphite film-coating powder...", cover Put the crucible cover in the heat treatment furnace;
[0053] 5) Vacuumize the heat treatment furnace and feed it with argon gas. Under the p...
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