High-nickel positive electrode material with uniform coating layer and preparation method of high-nickel positive electrode material
A positive electrode material and coating layer technology, which is applied in the field of high nickel positive electrode material and its preparation, can solve the problems of high requirements on equipment and raw materials, unfavorable large-scale production, complex coating method, etc., and achieves reduction of surface pH and residual Lithium, low equipment requirements, low cost effect
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[0053] Example 1
[0054] Add 1kg of deionized water with 16g of lithium hydroxide dissolved in a 1L beaker and high nickel cathode active material LiNi 0.80 Co 0.10 Mn 0.10 O 2 1kg, stirring speed 500r / min, wait to be evenly stirred. Add slowly (NH 4 ) 2 HPO 4 The stirring speed of 3.25g remains unchanged, and it is preferable to continue stirring for 20 min. Filter the obtained mixture, filter with a vacuum water pump, rinse with 20 mL of absolute ethanol, drain, and dry in a blast oven at 150°C for 3 hours to obtain dry materials, which are placed in a sagger and placed in a preheated muffle furnace Sintering reaction at 700℃ for 10h under oxygen atmosphere (oxygen concentration ≥80%). Slowly cooling, crushing and sieving to obtain a high nickel positive electrode material active material with a uniform coating layer.
Example Embodiment
[0055] Example 2
[0056] Add 1kg of deionized water with 16g of lithium hydroxide dissolved in a 1L beaker and high nickel cathode active material LiNi 0.90 Co 0.05 Mn 0.05 O 2 1kg, stirring speed 500r / min, wait to be evenly stirred. Add Na slowly 3 PO 4 The stirring speed of 4.03g remains unchanged, and it is preferable to continue stirring for 20 minutes. Filter the obtained mixture, filter with a vacuum water pump, rinse with 20 mL of absolute ethanol, drain, and dry in a blast oven at 150°C for 3 hours to obtain dry materials, which are placed in a sagger and placed in a preheated muffle furnace Sintering reaction at 700℃ for 10h under oxygen atmosphere (oxygen concentration ≥80%). Slowly cooled, crushed and sieved to obtain a high nickel cathode material active material LiNi with a uniform coating layer 0.90 Co 0.05 Mn 0.05 O 2 .
Example Embodiment
[0057] Example 3
[0058] Add 1kg of deionized water with 16g of lithium hydroxide dissolved in a 1L beaker and high nickel cathode active material LiNi 0.80 Co 0.10 Mn 0.10 O 2 1kg, stirring speed 500r / min, wait to be evenly stirred. Slowly join K 3 PO 4 The stirring speed of 5.22g remains unchanged, and it is preferable to continue stirring for 20 minutes. Filter the obtained mixture, filter with a vacuum water pump, rinse with 20 mL of absolute ethanol, drain, and dry in a blast oven at 150°C for 3 hours to obtain dry materials, which are placed in a sagger and placed in a preheated muffle furnace Sintering reaction at 700℃ for 10h under oxygen atmosphere (oxygen concentration ≥80%). Slowly cooled, crushed and sieved to obtain a high nickel cathode material active material LiNi with a uniform coating layer 0.80 Co 0.10 Mn 0.10 O 2 .
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