A kind of high bonding strength negative electrode slurry and preparation method thereof
A negative electrode slurry, high bonding technology, applied in electrode manufacturing, structural parts, battery electrodes, etc., can solve problems affecting battery life, exposed foil, negative electrode material drop, etc., to improve negative electrode material drop phenomenon, improve peeling Strength, the effect of improving process efficiency
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Embodiment 1
[0022] A high-bonding strength negative electrode slurry is made from the following raw materials by weight:
[0023] 95 parts of graphite, 2 parts of conductive agent, 1 part of styrene-butadiene emulsion, 1 part of oligoethylene oxide, 1 part of sodium carboxymethyl cellulose, 130 parts of deionized water; the conductive agent is a mixture of SP and KS6, And the weight ratio of SP and KS6 is 4:3; the solid content of styrene-butadiene emulsion is 40wt%, and the molecular weight of oligoethylene oxide is 2000;
[0024] The preparation method of the high bonding strength negative electrode slurry comprises the following steps:
[0025] S1, by weight, add 1 part of oligoethylene oxide and 50 parts of deionized water in the reactor, stir for 2 hours under the condition of vacuum tightness-0.09MPa, stirring speed 18 rev / min, add 1 part carboxymethyl cellulose sodium and 80 parts of deionized water, and continue to stir for 2 hours under the conditions of vacuum degree -0.09MPa a...
Embodiment 2
[0038] The high bonding strength negative electrode slurry proposed by the present invention, its raw materials include: negative electrode active material, binder, thickener, conductive agent and solvent; wherein, the binder is oligoethylene oxide and A mixture of styrene-butadiene emulsions.
Embodiment 3
[0040] The high bonding strength negative electrode slurry proposed by the present invention, its raw materials include: negative electrode active material, binder, thickener, conductive agent and solvent; wherein, the binder is oligoethylene oxide and A mixture of styrene-butadiene emulsions;
[0041] Among them, among the raw materials, the weight ratio of negative electrode active material, binder, thickener, conductive agent and solvent is 95:2:3:2:190;
[0042] The weight ratio of the oligoethylene oxide and the styrene-butadiene emulsion is 1:4, the solid content of the styrene-butadiene emulsion is 35 wt %, and the molecular weight of the oligoethylene oxide is 2000.
[0043] The present invention also proposes a method for preparing the high bonding strength negative electrode slurry, comprising the following steps:
[0044] S1. Mix the oligoethylene oxide with part of the solvent, stir and disperse for 2h, add thickener and the remaining solvent and continue to stir ...
PUM
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