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A kind of animal source amino acid liquid oil separation treatment process

A technology of oil separation and treatment process, which is applied in the direction of fat oil/fat production, fat oil/fat refining, fat production, etc. It can solve the problems of incomplete product separation and high processing cost, and achieve low equipment investment and operation costs and low processing costs , to avoid the effect of saponification or emulsification

Active Publication Date: 2022-06-28
沭阳利民畜禽无害化处理有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the disadvantages of high processing cost and incomplete product separation, the technology of reducing acid value of common oils and fats

Method used

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  • A kind of animal source amino acid liquid oil separation treatment process
  • A kind of animal source amino acid liquid oil separation treatment process
  • A kind of animal source amino acid liquid oil separation treatment process

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0023] A kind of animal source amino acid liquid oil separation processing technology, its processing technology comprises the following steps:

[0024] (1) Pretreatment of amino acid solution:

[0025] Weigh 25 parts of dead livestock and poultry, 0.45 parts of concentrated sulfuric acid and 8.2 parts of water into the reaction kettle, the stirring speed is 12r / min, the stirring temperature is 132 ℃, and the mixing reaction is carried out under the conditions of 0.12MPa for 5h, stop stirring, and control the pressure of the reaction kettle. At 0.03MPa for 2h, the amino acid solution was obtained;

[0026] (2) Grease separation process:

[0027] In step (1), the material and grease are discharged through the discharge port, the grease is pumped to the temporary storage tank, and hot steam is passed into the temporary storage tank, the stirring speed is 80 r / min, the stirring time is 5 min, and the water layer is separated by standing. Pump to the fertilizer water storage tan...

Embodiment 2

[0031] A kind of animal source amino acid liquid oil separation processing technology, its processing technology comprises the following steps:

[0032] (1) Pretreatment of amino acid solution:

[0033] Weigh 25 parts of dead livestock and poultry, 0.1 part of concentrated sulfuric acid and 2 parts of water into the reaction kettle, the stirring speed is 1r / min, the stirring temperature is 95 ° C, 0.01MPa under the conditions of mixing reaction for 8h, stop stirring, and control the pressure of the reaction kettle. At 0.01MPa for 5h, the amino acid solution was obtained;

[0034] (2) Grease separation process:

[0035] In step (1), the material and grease are discharged through the discharge port, the grease is pumped to the temporary storage tank, and hot steam is passed into the temporary storage tank, the stirring speed is 20 r / min, the stirring time is 3 min, and the water layer is separated by standing. Pump to the fertilizer water storage tank; repeat the above steam w...

Embodiment 3

[0039] A kind of animal source amino acid liquid oil separation processing technology, its processing technology comprises the following steps:

[0040] (1) Pretreatment of amino acid solution:

[0041] Weigh 25 parts of dead livestock and poultry, 6 parts of concentrated sulfuric acid and 10 parts of water into the reaction kettle, the stirring speed is 40r / min, the stirring temperature is 150 ℃, and the reaction is mixed for 1 hour under the conditions of 0.01MPa, the stirring is stopped, and the pressure of the reaction kettle is controlled. At 0.5MPa for 0.2h, the amino acid solution was obtained;

[0042] (2) Grease separation process:

[0043] In step (1), the material and grease are discharged through the discharge port, the grease is pumped to the temporary storage tank, and hot steam is passed into the temporary storage tank. Pump to the fertilizer water storage tank; repeat the above steam washing operation 5 times and centrifuge to obtain preliminary purified oil;...

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Abstract

The invention relates to a process for separating and treating animal source amino acid liquid oil. Including amino acid solution pretreatment, oil separation process and oil acid value reduction process. The process of the invention has the advantages of high oil-water separation efficiency of amino acid liquid, simple operation, low energy consumption, no waste water discharge, low acid value of oil and the like.

Description

technical field [0001] The invention relates to the field of harmless treatment of sick and dead livestock and poultry, in particular to an animal-derived amino acid liquid oil and fat separation and treatment process. Background technique [0002] With the rise of the harmless treatment of sick and dead livestock and poultry, the new acid hydrolysis process for the harmless treatment of livestock and poultry has been included in the technical specifications for harmless treatment, and the problem of post-treatment of products derived from this new process needs to be solved urgently. The conventional oil acid value treatment scheme is to add alkaline substances such as potassium hydroxide, sodium hydroxide, ammonia water to carry out acid-base neutralization. However, the by-products produced by this treatment process are prone to emulsification or saponification problems, which affect the separation of oil and by-products. ; The high temperature deacidification treatment p...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B09B1/00C11B1/16C11B3/00C11B3/10C11B3/16
CPCC11B1/16C11B3/001C11B3/008C11B3/16C11B3/10
Inventor 武传建卢南
Owner 沭阳利民畜禽无害化处理有限公司