A kind of LED illuminating lamp with low color temperature and low blue light radiation and preparation method thereof
A technology of LED lighting and low color temperature, applied in the field of LED lighting, can solve the problems of high color temperature and serious blue light radiation of LED light source, and achieve the effect of reducing the amount of blue light radiation, reducing the amount of blue light radiation, and fewer operating procedures
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Embodiment 1
[0034] Weigh 1.2514 g of zinc acetate dihydrate solid into a beaker, add 200 ml of ethanol, stir for 5 min, and ultrasonically shake for 10 min at 35 °C until the zinc acetate dihydrate solid is completely dissolved.
[0035] Pour the solution into a three-necked flask, condense and reflux in a digital temperature-controlled magnetic stirring oil bath at 80 °C for 2 h, pour it into a beaker and put it in a refrigerator at 4 °C for refrigeration until use; weigh 8.00 g of NaOH solid in Add 100 ml of ethanol to the beaker, stir for 10 min, and oscillate ultrasonically for 30 min at 35 °C until the solids are fully dissolved, then place it for use; take 100 ml of the precursor solution in a three-necked flask, heat it to 45 °C in a magnetic stirring oil bath, Use a syringe to quickly add 5.00 ml of the ethanol solution of NaOH above, react for 5 min, pour it into a beaker, and cool to room temperature for use; add 100 ml of n-hexane to the reaction solution, stir for 5 min, centri...
Embodiment 2
[0039] Weigh 1.2514 g of zinc acetate dihydrate solid into a beaker, add 200 ml of ethanol, stir for 5 min, and ultrasonically shake for 10 min at 35 °C until the zinc acetate dihydrate solid is completely dissolved.
[0040] Pour the solution into a three-necked flask, condense and reflux in a digital temperature-controlled magnetic stirring oil bath at 80 °C for 2 h, pour it into a beaker and put it in a refrigerator at 4 °C for refrigeration until use; weigh 8.00 g of NaOH solid in Add 100 ml of ethanol to the beaker, stir for 10 min, and oscillate ultrasonically for 30 min at 35 °C until the solid is fully dissolved, and set aside for use; take 100 ml of the precursor solution in a three-necked flask, heat it to 45 °C in a magnetic stirring oil bath, Use a syringe to quickly add 5.00 ml of the ethanol solution of NaOH above, react for 5 min, pour it into a beaker, and cool to room temperature for use; add 100 ml of n-hexane to the reaction solution, stir for 5 min, centrifu...
Embodiment 3
[0044]Weigh 1.2514 g of zinc acetate dihydrate solid into a beaker, add 200 ml of ethanol, stir for 5 min, and ultrasonically shake for 10 min at 35 °C until the zinc acetate dihydrate solid is completely dissolved.
[0045] Pour the solution into a three-necked flask, condense and reflux in a digital temperature-controlled magnetic stirring oil bath at 80 °C for 2 h, pour it into a beaker and put it in a refrigerator at 4 °C for refrigeration until use; weigh 8.00 g of NaOH solid in Add 100 ml of ethanol to the beaker, stir for 10 min, and oscillate ultrasonically for 30 min at 35 °C until the solids are fully dissolved, then place it for use; take 100 ml of the precursor solution in a three-necked flask, heat it to 45 °C in a magnetic stirring oil bath, Use a syringe to quickly add 5.00 ml of the ethanol solution of NaOH above, react for 5 min, pour it into a beaker, and cool to room temperature for use; add 100 ml of n-hexane to the reaction solution, stir for 5 min, centrif...
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