Method and device for measuring atomization particle size distribution and atomization rate of high-melting-point materials

A particle size distribution and measuring device technology, which is used in the measurement of atomization particle size distribution and atomization rate of high-melting point materials, and the measurement field of atomization particle size distribution and atomization rate, which can solve the problem that the overall spray field cannot be accurately measured. Atomization rate, difficult to identify droplets, errors and other problems, to achieve the effect of solving the overall atomization particle size distribution and the measurement accuracy of the atomization rate, high accuracy and low cost

Active Publication Date: 2019-09-06
HARBIN ENG UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

For example, the imaging method uses a high-speed camera to record the spray process, and then combines image processing software to calculate the atomization rate and droplet size distribution. The high area is not applicable; another method is to use a spray particle size analyzer to measure the particle size distribution of the atomization field. Its working principle is based on the principle of laser forward scattering. Scattering occurs, and the distribution of scattered light energy is related to the size of the particles. The forward scattered light energy distribution is measured by a specially designed and manufactured fan-shaped multi-element photodetector, and then the measured data is processed by an inversion algorithm to obtain the measured The particle size distribution of the particles, however, this method can only measure the droplet size distribution passing through a straight line at a time, and use the particle size distribution on a straight line to infer the overall distribution, that is, it is assumed that the distribution of the atomization field is axisymmetric However, in actual situations, there may be large differences in the distribution of droplet sizes in different radial directions, which will lead to large errors, and these two methods cannot accurately measure the overall atomization rate of the spray field

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  • Method and device for measuring atomization particle size distribution and atomization rate of high-melting-point materials
  • Method and device for measuring atomization particle size distribution and atomization rate of high-melting-point materials

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Embodiment 1

[0032] Embodiment 1. This embodiment provides a method for measuring the atomized particle size distribution and atomization rate of high melting point materials, which includes the following steps:

[0033] (1) Before the spray experiment, it is necessary to ensure the inert gas environment in the experiment to prevent the high melting point material from being oxidized during the spraying process; heat the material to the required temperature T 0 ; Set a collection dish filled with organic coolant in the lower part of the atomization field to collect the falling jets and atomized droplets.

[0034] (2) Use high-pressure inert gas to extrude high-melting-point materials in molten state, form jets and sprays through nozzles, and fall into organic coolant, spray droplets and jets will be rapidly cooled and solidified into particles and massive solids, deposited on the collector dish bottom.

[0035] (3) Separating the collected solid particles and massive solids, and weighing ...

Embodiment 2

[0040] This embodiment provides a device for measuring atomized particle size distribution and atomization rate of high melting point materials, which includes a closed container 1-8, a sealed crucible 1-6, a heating device 1-7, and a lower collecting vessel 1-14. The closed container 1-8 adopts a structure with a wide top and a narrow bottom. The plane formed in the middle is used to support the sealed crucible 1-6 located in the upper part of the container and the heating device 1-7 around it. The bottom of the crucible 1-6 is provided with an opening. For connection with different types of nozzles 1-11. The lower part of the airtight container 1-8 is connected with the collecting vessel 1-14, and the organic coolant 1-15 is housed in the collecting vessel 1-14, which is used to cool the sprayed liquid droplets into solid particles 1-13. The function of adjusting the distance between the liquid surface of the coolant 1-15 and the nozzle 1-11 is realized by connecting differe...

Embodiment 3

[0043] This embodiment takes liquid sodium as an example to illustrate the specific process of measuring the atomized particle size distribution and overall atomization rate of liquid sodium using the method proposed in the present invention.

[0044] 1. Preparatory work: Due to the active chemical properties of liquid sodium, it is necessary to ensure the inert gas environment in the experimental container before the spray test to prevent oxidative combustion of liquid sodium during the spraying process. Heat the sodium in sealed crucibles 1-6 to 300°C and select the nozzle. Set a collection dish 1-4 filled with liquid paraffin 1-3 at the bottom of the experimental container, adjust the height so that the liquid level of the paraffin remains at a position 2m away from the nozzle, and the temperature of the liquid paraffin is room temperature.

[0045] 2. Spray experiment and droplet solidification: The liquid sodium is injected from the nozzle with 2 atmospheres of argon, and...

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Abstract

The invention provides a method and device for measuring atomization particle size distribution and the atomization rate of high-melting-point materials. The device comprises a sealed container, a sealed crucible, heating devices, a collecting vessel and a pipeline adjusting device; the sealed crucible and the heating devices are arranged in the sealed container, the heating devices are arranged on the periphery of the sealed crucible, and the collecting vessel is connected with the lower part of the sealed crucible; the pipeline adjusting device comprises a main pipeline, a first branch pipeline, a second branch pipeline, an inflating hole and an exhaust hole, wherein the first branch pipeline and the second branch pipeline are connected with the main pipeline, and the inflating hole andthe exhaust hole are formed in the sealed container; the first branch pipeline communicates with the sealed container, and the second branch pipeline communicates with the sealed crucible; and a gas flowmeter is mounted on the main pipeline, and a pressure gauge is mounted on the second branch pipeline. All liquid drops in an atomization field are collected and cooled into solid particles, and theproblems that an existing method and device are insufficient in resolution ratio, and overall particle size distribution and atomization rate of the atomization field cannot be measured are solved successfully.

Description

technical field [0001] The invention relates to a method for measuring atomization particle size distribution and atomization rate, in particular to a method for measuring atomization particle size distribution and atomization rate of high melting point materials, and belongs to the field of research on atomization characteristics of high melting point materials. Background technique [0002] The fine metal powder produced by atomization pulverization technology is widely used in aviation, aerospace, ship, automobile, metallurgy and other fields, especially in some new fields of material preparation such as powder injection molding, self-propagating superalloy, metal Matrix composite materials are also based on fine metal powder. The atomization particle size distribution and atomization rate of metal spray are an important index of atomization powder making technology; in thermal spraying technology, it is necessary to use coating materials such as corrosion-resistant metal ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N15/02G01N5/00B22F9/08
CPCG01N15/0272G01N15/0227G01N5/00B22F9/082Y02P10/25
Inventor 张智刚马瑶龙王赟
Owner HARBIN ENG UNIV
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