Method for preparing large-area copper Cu(111) monocrystal
A single crystal, copper foil technology, applied in the field of materials, can solve problems such as limiting the application of copper foil
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[0038] In the first step, the 100 μm thick commercial copper foil (purity 99.9%) is cut into a size of about 4cm × 6cm, and electrochemically polished in an ethanol / phosphoric acid system (wherein, the specific composition of the polishing solution is: deionized water ( mL), phosphoric acid (mL), ethanol (mL), isopropanol (mL) and urea (g) were mixed according to the ratio of 250:125:125:25:4; the conditions of electrochemical polishing were: the holding voltage was 5V, the current is 2A, and the polishing time is 3min.) Wash with deionized water to remove residual polishing liquid on the surface, and blow dry with nitrogen.
[0039] In the second step, the copper foil obtained in the first step is placed in a high-temperature tube furnace, and 200 sccm of argon gas and 100 sccm of hydrogen gas are introduced to start heating. The temperature of the tube furnace was raised to 1075°C, and the heating time was 45 minutes. Hold for 1h for annealing. After cooling down to room t...
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