Silicate aqueous solution, fertilizer, preparation method of the fertilizer and carbonized powder for preparing silicate aqueous solution or fertilizer
An aqueous solution and silicate technology, applied in inorganic fertilizers, potash fertilizers, applications, etc., can solve the problems of difficult removal of organic matter, high time cost and high time, and achieve the effect of reducing the reaction time, speeding up the reaction speed and promoting the reaction.
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preparation example 1
[0120] Preparation of Purified Powder
[0121] The purified powder of Preparation Example 1 is obtained by the following steps:
[0122] Step (1): Provide a silicon filter cake containing silicon, water and organic matter. The silicon filter cake is the cutting silicon powder (D 50 -The particle size is 0.8μm) aqueous solution is prepared by plate and frame filter press after plate and frame filter press. Wherein, based on the total weight of the silicon filter cake as 100wt%, the content of water is 40wt%.
[0123] Step (2-1): Dewatering the silicon filter cake in a vacuum oven at 160° C. to obtain a dehydrated silicon filter cake after the solid content in the silicon filter cake is 99-99.5 wt%.
[0124] Step (2-2): After pulverizing the dewatered filter cake with a crusher, a plurality of D 50 Reactive particles with a particle size of 1 mm and containing silicon and organic matter.
[0125] Step (2-3): first remove the organic matter in the reaction particles, and th...
preparation example 2
[0127] Preparation of Purified Powder
[0128] The purified powder of Preparation Example 2 is made by the following steps:
[0129] Step (1): Same as Step (1) of Preparation Example 1.
[0130] Step (2-1): first mix the silicon filter cake with reverse osmosis water (RO water), stir and disperse through a high-speed mixer, and then filter through a 150-mesh sieve to obtain a mixed solution. Wherein, after stirring and dispersing and before filtering, based on the total weight of the solution as 100wt%, the weight of the powder formed by the silicon filter cake is 20wt%.
[0131] Step (2-2): After spray-drying the mixed solution, a plurality of D 50 Black reactive particles with a diameter of 36.11 μm, containing silicon and organic matter, and spherical in shape. Among them, the method of spray drying is to transport the mixed solution to the centrifugal atomizing nozzle with a quantitative pump at a feed rate of 40g per minute, and after the mixed solution is centrifugal...
preparation example 3
[0134] Preparation of Purified Powder
[0135] The purified powder of Preparation Example 3 is obtained by the following steps:
[0136] Step (1): Same as Step (1) of Preparation Example 1.
[0137] Step (2-1): After kneading and air-drying the silicon filter cake in a kneading dryer (temperature is 150° C.; pressure is air-exhaust to -70 cmHg), a plurality of D 50 Reactive particles with a particle size of 2.58 μm and irregular shapes. It needs to be explained again that each reaction particle is composed of multiple D 50 It is composed of primary particles with a particle size of 0.8 μm and containing silicon and organic matter.
[0138] Step (2-2): removing the organic matter in the reaction particles to obtain a purified powder. Wherein, the purified powder includes a plurality of D 50 Irregular secondary particles with a particle size of 2.5 μm, and each secondary particle is composed of multiple D 50 Consists of silicon-containing primary particles with a particle...
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