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Preparation method of sodium butyrate granules and tail gas treatment method thereof

A technology of tail gas treatment and sodium butyrate, which is applied to the method of granulating raw materials, carboxylate preparation, carboxylate preparation, etc., can solve the problems of easy moisture absorption, sour odor, high transportation cost, and easy generation of dust, etc. , to achieve the effect of easy reaction, advanced drying technology, and realization of recycling

Inactive Publication Date: 2019-11-01
日照东润德农牧发展有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The original powder type sodium butyrate product is a 60-120-mesh powder with a small specific gravity, large volume during transportation, and high transportation costs; during use, it is easy to generate dust, easy to absorb moisture, and has a sour smell of rotten cheese. Easy to use, some powder will be sucked away by the induced air system during processing

Method used

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  • Preparation method of sodium butyrate granules and tail gas treatment method thereof
  • Preparation method of sodium butyrate granules and tail gas treatment method thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0036] A kind of sodium butyrate granule preparation method of the present invention and tail gas treatment method thereof are as follows:

[0037] Preparation of S1 sodium butyrate raw material: neutralize n-butyric acid and ionic membrane liquid caustic soda to obtain sodium butyrate reaction liquid, after drying the sodium butyrate reaction liquid through the spray drying system, directly from the bottom of the spray drying system The crude product of sodium butyrate with a water content of 5.5wt% is obtained by flowing out, and the powdery material is collected from the position above the bottom of the spray drying system through the air delivery system, and the finished product is directly packaged;

[0038] S2 mixing: the sodium butyrate crude product with a water content of 5.5 wt% obtained in step S1 is mixed with water, and mixed uniformly by a mixer equipped with a high-speed cutting coulter;

[0039] S3 extruding: the material mixed in step S2 is evenly added into t...

Embodiment 2

[0050] A kind of sodium butyrate granule preparation method of the present invention and tail gas treatment method thereof are as follows:

[0051] Preparation of S1 sodium butyrate raw material: neutralize n-butyric acid and ionic membrane liquid caustic soda to obtain sodium butyrate reaction liquid, after drying the sodium butyrate reaction liquid through the spray drying system, directly from the bottom of the spray drying system The crude product of sodium butyrate with a water content of 3wt% is obtained from the outflow, and the powdery material is collected from the position above the bottom of the spray drying system through the air delivery system, and the finished product is directly packaged;

[0052] S2 mixing: the sodium butyrate crude product with a water content of 3wt% obtained in step S1 is mixed with water, and mixed uniformly by a mixer equipped with a high-speed cutting coulter;

[0053] S3 extruding: the material mixed in step S2 is evenly added into the ...

Embodiment 3

[0064] A kind of sodium butyrate granule preparation method of the present invention and tail gas treatment method thereof are as follows:

[0065] Preparation of S1 sodium butyrate raw material: neutralize n-butyric acid and ionic membrane liquid caustic soda to obtain sodium butyrate reaction liquid, after drying the sodium butyrate reaction liquid through the spray drying system, directly from the bottom of the spray drying system The crude product of sodium butyrate with a water content of 8wt% is obtained by flowing out, and the powdery material is collected from the position above the bottom of the spray drying system through the air delivery system, and the finished product is directly packaged;

[0066] S2 mixing: mixing the sodium butyrate crude product with a water content of 8wt% obtained in step S1 with water, and mixing uniformly with a mixer equipped with a high-speed cutting coulter;

[0067] S3 extruding: the material mixed in step S2 is evenly added into the e...

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Abstract

The invention provides a preparation method of sodium butyrate granules and a tail gas treatment method of the sodium butyrate granules. The invention relates to the field of preparation of non-antibiotic growth-promoting feed additives. The preparation method mainly comprises the following steps: preparing a sodium butyrate raw material, mixing the components, extruding the mixture into strips, granulating the mixture, and performing shot blasting and drying. The invention also relates to the treatment method for tail gas in preparation of the sodium butyrate granules. The treatment method comprises the following steps: collecting tail gas obtained by spray drying, treating the tail gas through a heat exchanger so as to collect heat in the tail gas, and then treating the cooled tail gas through a two-stage water film scrubber tower so as to obtain clean tail gas; and finally, performing heat exchange through the heat exchanger, and compensating heat for the storage tank through the jacket and discharging the residual clean gas. The preparation method of the sodium butyrate granules is safe, simple, convenient, good in controllability, environment-friendly and reliable.

Description

technical field [0001] The invention relates to the field of preparation of non-antibiotic growth-promoting feed additives, in particular to a preparation method of sodium butyrate granules and a tail gas treatment method thereof. Background technique [0002] With the promulgation and implementation of new feed regulations, the use of antibiotics in feed additives, feed and breeding industries has been completely banned. Sodium butyrate raw powder (feed additive) as an antibiotic substitute has been approved in the feed and breeding industries after years of development, and its usage is increasing. The original powder type sodium butyrate product is a 60-120-mesh powder with a small specific gravity, large volume during transportation, and high transportation costs; during use, it is easy to generate dust, easy to absorb moisture, and has a sour smell of rotten cheese. It is easy to use, and part of the powder will be sucked away by the induced air system during the proce...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J2/20B01J2/00B01D53/78B01D53/75B01D53/72B01D47/00B01D1/18A23K40/10A23K20/22A23K20/105F26B3/08C07C51/41C07C53/124
CPCA23K20/105A23K20/22A23K40/10B01D1/18B01D47/00B01D53/72B01D53/75B01D53/78B01J2/00B01J2/20C07C51/412F26B3/08F26B2200/08C07C53/124
Inventor 郭衍涛陈守慧赵仲昌郝永任贾衍俊
Owner 日照东润德农牧发展有限公司
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