Ionic conductive electrochemical luminescent hydrogel for luminescent displayerand preparation method of ionic conductive electrochemical luminescent hydrogel
An ion-conducting and electrochemical technology, applied in chemical instruments and methods, luminescent materials, organic chemistry, etc., can solve problems such as inability to effectively fix the medium, easy diffusion and loss of the medium, affecting display performance, etc. The effect of low initiation voltage and low fabrication cost
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Embodiment 1
[0041] 1) Use a balance to weigh 0.1564g of AM, 0.02g of MBAA and 0.0362g of NaAA, dissolve the weighed solid powder (AM, MBAA, NaAA) in 500μL of deionized water in sequence, shake and mix at room temperature for 2 to 3 minutes to obtain Colorless clear solution.
[0042] 2) Weigh 0.0037g of Ru(bpy) with a balance 3 Cl 2 , 0.0072g of TPA and 0.0292g of NaCl, the weighed material (Ru(bpy) 3 Cl 2 , TPA, NaCl) were sequentially added to the colorless clear solution of the above 1) and shaken and mixed at room temperature for 2 to 3 minutes to obtain a red transparent solution.
[0043] 3) Add 0.0009 g of APS and 0.0078 g of TEMED to the red transparent solution in 2), shake and mix at room temperature for 2 to 3 minutes to fully dissolve and add water to a total volume of 1 mL to obtain the final mixed solution.
[0044] 4) After the final mixed solution was allowed to stand at room temperature for 60 minutes, the target hydrogel ( figure 2 ).
[0045] The target hydrogel ...
Embodiment 2
[0050] 1) Weigh 0.1564g of AM, 0.02g of MBAA and 0.0362g of NaAA with a balance, dissolve the above-mentioned solid powders (AM, MBAA, NaAA) in sequence in 500μL of deionized water, shake and mix at room temperature for 2 to 3 minutes A colorless clear solution was obtained.
[0051] 2) Weigh 0.0008g of Ru(bpy) with a balance 3 Cl 2 , 0.0014g of TPA and 0.0292g of NaCl, the weighed material (Ru(bpy) 3 Cl 2 , TPA, NaCl) were sequentially added to the colorless clear solution of the above 1) and shaken and mixed at room temperature for 2 to 3 minutes to obtain a red transparent solution.
[0052] 3) Add 0.0009 g of APS and 0.0078 g of TEMED to the red transparent solution in 2), shake and mix at room temperature for 2 to 3 minutes to fully dissolve and add water to a total volume of 1 mL to obtain the final mixed solution.
[0053] 4) The final mixed solution was left to stand at room temperature for 60 minutes to obtain a red transparent hydrogel.
[0054] After identifica...
Embodiment 3
[0057] 1) Weigh 0.1564g of AM, 0.02g of MBAA and 0.0362g of NaAA with a balance, dissolve the above-mentioned solid powders (AM, MBAA, NaAA) in sequence in 500μL of deionized water, shake and mix at room temperature for 2 to 3 minutes A colorless clear solution was obtained.
[0058] 2) Weigh 0.0037g of Ru(bpy) with a balance 3 Cl 2 , 0.0072g of TPA and 0.0058g of NaCl, the weighed material (Ru(bpy) 3 Cl 2 , TPA, NaCl) were sequentially added to the colorless clear solution of the above 1) and shaken and mixed at room temperature for 2 to 3 minutes to obtain a red transparent solution.
[0059] 3) Add 0.0009 g of APS and 0.0078 g of TEMED to the red transparent solution in 2), shake and mix at room temperature for 2 to 3 minutes to fully dissolve and add water to a total volume of 1 mL to obtain the final mixed solution.
[0060] 4) The final mixed solution was heated in an oven at 60° C. for 30 minutes to obtain a red transparent hydrogel.
[0061] After identification, ...
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