Color change cellulose fiber preparation method
A cellulose fiber, temperature-sensitive discoloration technology, applied in the textile field, can solve the problems of unsustainable discoloration effect, poor stability of temperature-sensitive discoloration materials, etc., and achieves the effects of stable performance, easy coating, and improved discoloration durability.
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Embodiment 1
[0042] (1) Preparation of color-changing microcapsule slurry
[0043] The capsule core material in the color-changing microcapsules is composed of temperature-sensitive color-changing material and luminous material. The temperature-sensitive color-changing material is composed of 3,6-diethoxyfluorane, boric acid and myristyl alcohol, and the luminous material is SrAl, a long-lasting afterglow material. 2 o 4 : Eu, Dy; the mass ratio of 3,6-diethoxyfluorane, boric acid and myristyl alcohol in the thermochromic material is 1:2:30.
[0044] The specific preparation method of the capsule core material is to mix 3,6-diethoxyfluorane and luminous material in a mass ratio of 1:1, grind in a grinder until the particle size is less than 100nm, and then mix it with boric acid and myristyl alcohol evenly , to obtain the capsule core material;
[0045] The wall material of the microcapsules is polymethyl methacrylate, the mass ratio of the wall material of the microcapsules to the core ...
Embodiment 2
[0051] (1) Preparation of color-changing microcapsule slurry
[0052] The capsule core material in the color-changing microcapsules is composed of temperature-sensitive color-changing material and luminous material. The temperature-sensitive color-changing material is composed of crystal violet lactone, bisphenol A and cetyl alcohol, and the luminous material is long afterglow material CaAl 2 o 4 : Eu, Nd; the mass ratio of crystal violet lactone, bisphenol A and cetyl alcohol in the thermochromic material is 1:3:50.
[0053] The preparation method of the capsule core material is to mix crystal violet lactone and luminous material at a mass ratio of 2:1, grind them in a grinder until the particle size is less than 100nm, and then mix them with bisphenol A and cetyl alcohol to prepare the capsule core Material;
[0054] Melamine-formaldehyde resin was selected as the capsule wall material, and the mass ratio of microcapsule capsule wall material to capsule core material was 1...
Embodiment 3
[0060] (1) Preparation of color-changing microcapsule slurry
[0061] The capsule core material in the color-changing microcapsules is composed of temperature-sensitive color-changing materials and luminous materials. The temperature-sensitive color-changing materials are composed of crystal violet lactone, bisphenol A and stearyl alcohol. The luminous material is long afterglow material MgSiO 3 : Mn, Eu, Dy; the mass ratio of crystal violet lactone, bisphenol A and stearyl alcohol in the thermochromic material is 1:4:40.
[0062] The preparation method of the capsule core material is to mix crystal violet lactone and luminous material at a mass ratio of 3:1, grind in a grinder until the particle size is less than 100nm, and then mix it evenly with bisphenol A and stearyl alcohol.
[0063] Urea-formaldehyde resin was selected as the capsule wall material, and the mass ratio of microcapsule capsule wall material to capsule core material was 1:1. Microcapsule slurry with a parti...
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