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Lubricating oil composition and preparation method thereof

A technology of lubricating oil composition and mineral oil, applied in the field of lubricating oil, can solve the problems of inability to dissipate heat in time, slow running speed, inconvenient oil change operation, etc.

Inactive Publication Date: 2020-01-17
CHINA PETROLEUM & CHEM CORP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The grinding roller is the key component of the vertical mill. Due to the large load and slow running speed of the grinding roller bearing, ordinary industrial closed gear oil with a viscosity level of ISO VG320-680 is often used for circulating lubrication. However, the disadvantage of using circulating lubrication is that the equipment investment , site occupancy, lubrication management costs are high
At present, users tend to choose the oil bath lubrication method to solve the above problems, but because the heat generated by the friction of the grinding roller during oil bath lubrication cannot be dissipated in time, the operating temperature of the lubricating oil is usually as high as 80-90°C, and there are high requirements for the assembly accuracy of the grinding roller bearings , Inconvenient oil change operation and other characteristics of use, if the use of ordinary gear oil cannot meet the requirements of ensuring sufficient oil film thickness and long oil change intervals at high temperatures, choosing a fully synthetic gear oil with good high temperature resistance will be expensive and lubricating oil consumption high cost problem

Method used

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  • Lubricating oil composition and preparation method thereof
  • Lubricating oil composition and preparation method thereof
  • Lubricating oil composition and preparation method thereof

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preparation example Construction

[0055] The present invention also provides a method for preparing the lubricating oil composition described above, comprising the following steps:

[0056] A) Stir the base oil at a vacuum degree of -0.090 to -0.095MPa and a temperature of 75 to 85°C to obtain a dehydrated base oil;

[0057] B) Mix the dehydrated base oil with the viscosity index improver at 60-70°C to obtain a hot mixture; or cool down the dehydrated base oil and mix it with the dilution of the viscosity index improver at 60-70°C , to obtain a hot mixture;

[0058] C) stirring and mixing the hot mixed liquid with antioxidant, extreme pressure antiwear agent, corrosion inhibitor and antifoaming agent at 55-65° C., and cooling to obtain a lubricating oil composition.

[0059] In the preparation method of the lubricating oil composition provided by the present invention, the raw material components and proportions used are the same as above, and will not be repeated here.

[0060] In the invention, the base oi...

Embodiment 1

[0080] Weigh medium viscosity polyalphaolefin oil PAO20 (40°C kinematic viscosity 190mm 2 / s) 5.0kg and 120BS bright stock 76.56kg, pour the two into the container, stir at -0.095MPa vacuum degree, 85℃ temperature for 1h for dehydration treatment. The temperature was lowered to 70° C., and 16.5 kg of polyisobutylene was added dropwise (dropping rate: 250 L / h) with stirring to obtain a hot mixed liquid. Remove the vacuum, lower the temperature to 65°C, add 0.5kg of polymethyl methacrylate, 0.9kg of sulfurized isobutylene, 0.135kg of C13 tertiary alkylamine, 0.072kg of C8 alkyl phosphite, 0.036kg of diisooctyl phosphate, monophosphate Isooctyl ester 0.036kg, C18 alkanol borate 0.036kg, C18 enamine 0.0315kg, finally add 0.01kg of 5000# methyl silicone oil dilution (the quality of 5000# methyl silicone oil in the 5000# methyl silicone oil dilution is 0.001 kg, 5000# methyl silicone oil and kerosene are mixed uniformly at a mass ratio of 1:9 to obtain 5000# methyl silicone oil dilu...

Embodiment 2

[0082] Weigh medium viscosity polyalphaolefin oil PAO40 (40°C kinematic viscosity 400mm 2 / s) 15kg and 70.06kg of 150BS bright stock, pour the two into the container, stir at -0.090MPa vacuum, 75°C for 0.5h for dehydration. The temperature was lowered to 60° C., and 13 kg of polyisobutylene was added dropwise (dropping rate: 200 L / h) with stirring to obtain a hot mixed liquid. Remove the vacuum, lower the temperature to 55°C, add 0.5kg of polymethyl methacrylate, 0.9kg of sulfurized isobutylene, 0.135kg of C13 tertiary alkylamine, 0.072kg of C8 alkyl phosphite, 0.036kg of diisooctyl phosphate, monophosphate Isooctyl ester 0.036kg, C18 alkanol borate 0.036kg, C18 enamine 0.0315kg, finally add 0.01kg of 5000# methyl silicone oil dilution (the quality of 5000# methyl silicone oil in the 5000# methyl silicone oil dilution is 0.001 kg, 5000# methyl silicone oil and kerosene are mixed uniformly at a mass ratio of 1:9 to obtain 5000# methyl silicone oil dilution). Stir at a constan...

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Abstract

The invention relates to the technical field of lubricating oil, in particular to a lubricating oil composition and a preparation method thereof. The lubricating oil composition comprises the following components in parts by weight: 56-90 parts of base oil, 10 to 22 parts of a viscosity index improver, 0-1 part of a pour point depressant, 1-2 parts of an extreme-pressure anti-wear agent, 0.05 to 0.25 part of an antioxidant, 0.01-0.4 part of a corrosion inhibitor, and 0.0005-0.0015 part of an anti-foaming agent, wherein the base oil comprises mineral oil and synthetic oil; the kinematic viscosity of the mineral oil at 40 DEG C is 80-660 mm<2> / s; and the kinematic viscosity of the synthetic oil at 40 DEG C is 170-1500 mm<2> / s. According to the invention, the mineral oil and synthetic oil with specific viscosity are matched with other components to achieve a synergistic effect, and the finally obtained lubricating oil composition can be used for a vertical mill grinding roller bearing oilbath and has relatively excellent viscosity-temperature characteristics, oxidation resistance and extreme-pressure wear resistance.

Description

technical field [0001] The invention relates to the technical field of lubricating oil, in particular to a lubricating oil composition and a preparation method thereof. Background technique [0002] Vertical mill is a large industrial grinding equipment. Its working principle is to drive the grinding disc to rotate through the drive motor and reducer, the material falls from the feeding port to the center of the grinding disc, moves to the edge of the grinding disc under the action of centrifugal force and is crushed by the grinding roller, and the crushed material overflows from the edge of the grinding disc, and at the same time It is brought into the high-efficiency powder classifier by the high-speed upward hot air flow from the air ring, and the coarse powder is sorted and then returned to the grinding disc for re-grinding. Coarse materials that are not carried by the hot air flow settle from the air ring, and are fed into the mill through the bucket elevator of the ex...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C10M169/04C10M171/02C10N40/02C10N30/08C10N30/10C10N30/06
CPCC10M169/044C10M171/02C10M2203/1006C10M2205/02C10M2205/0206C10M2209/08C10M2215/04C10M2219/102C10M2223/04C10M2223/049C10M2227/061C10M2229/041
Inventor 龙胜前李姝熊瑶欧阳睿熙
Owner CHINA PETROLEUM & CHEM CORP
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