Regenerated cellulose fiber containing shea butter, and preparation method thereof
A technology of regenerated cellulose and shea butter, applied in the textile field, can solve the problems of non-applicable anti-fabric, etc., and achieve the effect of improving moisturizing performance
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Embodiment 1
[0044] Fibers were prepared as follows:
[0045] (1) The emulsification includes adding shea butter to the emulsifier, heating up to 35° C., and stirring at 3500 rpm for 30 min to obtain a shea butter emulsion; the mass ratio of the shea butter to the emulsifier is 1:0.5, the emulsifier is a mixture of polyethoxylated isotridecanol and Tween 80, and the mass ratio of polyethoxylated isotridecyl alcohol to Tween 80 is 0.3:1;
[0046] (2) Mix a certain proportion of melamine and formaldehyde, add deionized water to stir and adjust the pH to 8.0, slowly raise the temperature to 65°C, and stir at 1000rpm for 30min to obtain a prepolymer;
[0047] (3) Add the prepolymer prepared in step (2) dropwise to the shea butter emulsion prepared in step (1), while applying stirring with a rotating speed of 1300rpm, while adjusting the temperature to 60°C and adjusting the pH to 6.0, stir for 2 hours, add sodium methylene bis-naphthalene sulfonate to obtain microcapsule liquid;
[0048] (4)...
Embodiment 2
[0053] Fibers were prepared as follows:
[0054] (1) The emulsification includes adding shea butter to the emulsifier, heating up to 52° C., and stirring at 3100 rpm for 10 min to obtain a shea butter emulsion; the mass ratio of the shea butter to the emulsifier is 1:0.4, the emulsifier is a mixture of polyethoxylated isotridecanol and Tween 80, and the mass ratio of polyethoxylated isotridecyl alcohol to Tween 80 is 0.4:1;
[0055] (2) Mix a certain proportion of melamine and formaldehyde, add deionized water to stir and adjust the pH to 7.8, slowly raise the temperature to 65°C, and stir at a speed of 900rpm for 30min to obtain a prepolymer;
[0056] (3) Add the prepolymer prepared in step (2) dropwise to the shea butter emulsion prepared in step (1), while applying stirring with a rotating speed of 1300rpm, while adjusting the temperature to 60°C and adjusting the pH to 4.5, stir for 1 hour, add sodium methylene bis-naphthalene sulfonate to obtain microcapsule liquid;
[...
Embodiment 3
[0062] Fibers were prepared as follows:
[0063] (1) The emulsification includes adding shea butter to the emulsifier, heating up to 45° C., and stirring at 3000 rpm for 20 min to obtain a shea butter emulsion; the mass ratio of the shea butter to the emulsifier is 1:0.5, the emulsifier is a mixture of polyethoxylated isotridecanol and Tween 80, and the mass ratio of polyethoxylated isotridecyl alcohol to Tween 80 is 0.5:1;
[0064] (2) Mix a certain proportion of melamine and formaldehyde, add deionized water to stir and adjust the pH to 8.2, slowly raise the temperature to 65°C, and stir at 800rpm for 30min to obtain a prepolymer;
[0065] (3) Add the prepolymer prepared in step (2) dropwise to the shea butter emulsion prepared in step (1), while applying stirring at a speed of 1500 rpm, while adjusting the temperature to 60°C and adjusting the pH to 5. Stir for 30 minutes, add sodium methylene bis-naphthalene sulfonate to obtain microcapsule liquid;
[0066] (4) butylmeth...
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