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Device and process for recovery of low-grade waste heat of rectification system

The technology of a waste heat recovery device and a rectification system is applied in the field of low-grade waste heat recovery devices of a rectification system, which can solve the problems that the low-grade latent heat cannot be directly reused, the waste heat cannot be reused, and the leakage points are increased. High degree of equipment integration and the effect of reducing leakage points

Pending Publication Date: 2020-02-07
浙江省天正设计工程有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] Some rectification waste heat recovery technologies that use the latent heat of the overhead steam often introduce the overhead steam into other devices such as the concentration evaporator as a heat source. Although a large part of the waste heat can be recovered, the actual use is relatively low temperature. Grade waste heat
This direct recycling method has restrictions on the temperature requirements of other devices, and there are safety risks in the direct use of flammable and explosive tower top steam, and the introduction of materials into other devices also increases leakage points
[0005] Since the temperature of the steam at the top of the tower is lower than that of the reboiler at the bottom of the tower, a large amount of low-grade latent heat in the steam at the top of the tower cannot be directly recycled to the bottom reboiler
At the same time, if there are no other devices that require relatively low-grade heat sources nearby, this part of waste heat cannot be recycled

Method used

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  • Device and process for recovery of low-grade waste heat of rectification system
  • Device and process for recovery of low-grade waste heat of rectification system
  • Device and process for recovery of low-grade waste heat of rectification system

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0044] 50wt% benzene / toluene components are separated by rectification, and the feed rate of rectification raw materials is 10t / h. When the traditional rectification method is used for separation, the condensing water consumption of the top evaporative condenser and the material cooler is 415.51t / h, and the amount of high-temperature water vapor used for heating the reboiler of the tower kettle is 4.48t / h.

[0045] When adopting the rectification system low-grade waste heat recovery process of the present invention to separate, the intermediate heat exchange working medium is selected water, the cooling medium of the working medium cooler 4e and the still material cooler 4c are all selected circulating water, and the working medium evaporator 2b The heat medium is steam, the working medium compressor 3a pressurizes and discharges high-temperature and high-pressure steam with a temperature of 152°C and a pressure of 0.4MPa, and the total consumption of circulating water for th...

Embodiment 2

[0047] The 50wt% ethanol / water component is rectified and separated, and the feed rate of the rectified raw material is 10t / h. When the traditional rectification method is used for separation, the condensing water consumption of the top evaporative condenser and the material cooler is 1572.44t / h, and the amount of high-temperature water vapor used to heat the reboiler of the tower kettle is 16.42t / h.

[0048] When adopting the rectification system low-grade waste heat recovery process of the present invention to separate, the intermediate heat exchange working medium is selected dichloromethane, the refrigerant medium of the working medium cooler 4e and the still material cooler 4c are all selected circulating water, and the working medium evaporator The heat medium of 2b is water vapor, the working medium compressor 3a pressurizes and discharges high-temperature and high-pressure steam with a temperature of 95°C and a pressure of 0.4MPa, and the total consumption of circulat...

Embodiment 3

[0050] The 5wt% chlorofluoroethylene / R142b component is rectified and separated, and the feed rate of the rectified raw material is 10t / h. When the traditional rectification method is used for separation, the amount of frozen brine condensed by the top evaporative condenser and the feed cooler is 9.72t / h, and the amount of hot water used for heating the reboiler of the tower kettle is 11.19t / h h.

[0051] When adopting the low-grade waste heat recovery process of the rectification system of the present invention to separate, the intermediate heat exchange working medium is selected from fluorodichloromethane, the refrigerant medium of the working medium cooler 4e and the still material cooler 4c are all selected frozen brine, and the working medium The heat medium of the evaporator 2b is hot water, the working medium compressor 3a pressurizes and discharges high-temperature and high-pressure steam with a temperature of 59°C and a pressure of 0.4MPa, and the total amount of fro...

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Abstract

The invention discloses a device and process for recovery of low-grade waste heat of a rectification system. The device comprises a rectification tower, a tower top evaporation condenser, a raw material preheater, a tower kettle reboiler and a waste heat recovery system, wherein the waste heat recovery system comprises an intermediate heat-exchange working-medium vaporization device and a workingmedium compressor, all the tower top evaporation condenser, the raw material preheater and the tower kettle reboiler are heat exchangers, and an intermediate heat-exchange working medium is introducedinto a cold fluid inlet of the tower top evaporation condenser; a cold fluid outlet of the tower top evaporation condenser is connected with an air inlet of the working medium compressor through theintermediate heat-exchange working-medium vaporization device by using pipelines, an air outlet of the working medium compressor is connected with a hot fluid inlet of the tower kettle reboiler by using pipelines, and a hot fluid outlet of the tower kettle reboiler is connected with a hot fluid inlet of the raw material preheater through a pipeline; and the intermediate heat exchange working medium which is obtained after cooling is performed through heat exchange is discharged from the hot fluid outlet of the raw material preheater. The device has a simple structure, and low-grade heat of steam in the tower top of the rectification tower can be recovered effectively through the device.

Description

technical field [0001] The invention relates to a low-grade waste heat recovery device and process of a rectification system. Background technique [0002] Distillation is a technology that separates components in a mixture by utilizing their different volatilities. It is an important unit operation in petrochemical, pharmaceutical and other industries. With the rapid development of the chemical industry, the application of rectification operations is becoming more and more widespread; however, the energy consumption of the rectification process is very high, accounting for 50% to 70% of the energy consumption of the separation process in the entire chemical industry. Most of the energy consumed in the rectification process is not used for component separation, but is taken away by cooling water or materials. Therefore, the energy saving potential of the rectification process is great. Reasonable use of the heat energy of the rectification process itself can reduce the energ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01D3/14B01D3/32F25B27/02
CPCB01D3/14B01D3/32F25B27/02Y02A30/274Y02P70/10
Inventor 杨森顾川川吴晓军赵志明陈杰
Owner 浙江省天正设计工程有限公司
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