A method for preventing and controlling the phytotoxicity of crops by carbon nanotubes by residual herbicides
A carbon nanotube and multi-wall carbon nanotube technology, applied in the field of herbicides, can solve problems such as phytotoxicity, and achieve the effects of crop growth promotion, strong adsorption capacity, and good repair effect
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[0034] 1. The adsorption of MWCNTs to sulfentrazone / quinclorac is detected, and an adsorption isotherm is established; it specifically includes the following steps:
[0035] 1) Prepare standard solution of sulfentrazone: 2, 4, 8, 16, 32mg / L, standard solution of quinclorac: 0.1, 0.4, 1.6, 6.4, 25.6mg / L, set 3 repetitions for each concentration, Measure the peak area with a high performance liquid chromatograph, and establish a concentration-peak area coordinate system;
[0036] The chromatographic detection conditions for sulfentrazone are:
[0037] Column: 4.6mm(id)×250mm, Eclipse XDB-C18, particle size 5μm)
[0038] Mobile phase: methanol: water (0.1% formic acid) = 70:30
[0039] Flow rate: 1mL·min -1
[0040] Detection wavelength: 240nm
[0041] Injection volume: 10μL
[0042] Column temperature: 30℃
[0043] According to the regression equation fitted by the results of HPLC detection, Y represents the peak area, x represents the concentration of sulfentrazone,
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