Ammonia-free environment-friendly medium-phosphorus chemical nickel plating solution and preparation method thereof
An electroless nickel plating solution, an environmentally friendly technology, applied in the field of electroless plating, can solve problems such as increased production costs, unqualified products, dull coating surface, etc., achieve good high temperature resistance and improve performance
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[0038] The second aspect of the present invention provides a method for preparing an ammonia-free and environmentally friendly phosphorous electroless nickel plating solution. The steps include: dissolving nickel sulfate and an organic acid in water, adding sodium hypophosphite, sodium acetate, heat-stable grade Lactic acid, wetting agent, intermediate until well mixed.
[0039] The third aspect of the present invention provides an electroless plating method, which includes immersing the product to be treated in a nickel plating solution for electroplating, and the nickel plating solution is the above-mentioned ammonia-free and environmentally friendly phosphorous electroless nickel plating solution.
Embodiment 1
[0043] Embodiment 1 provides a kind of non-ammonia environment-friendly phosphorus electroless nickel plating liquid and preparation method thereof, by weight, comprising 40 parts of heat-stable grade lactic acid, 700 parts of nickel sulfate, 75 parts of organic acid, 35 parts of sodium acetate, times 120 parts of sodium phosphate, 0.02 parts of wetting agent, and 0.08 parts of intermediate.
[0044] The heat-stable lactic acid is 88% lactic acid;
[0045] The organic acid is a mixture of 2-hydroxysuccinic acid and succinic acid; the 2-hydroxysuccinic acid is 44wt% of the organic acid;
[0046] Described wetting agent is sodium 2-ethylhexyl sulfate;
[0047] The intermediate is butynediol diethoxy ether.
[0048]The preparation method of the phosphorous electroless nickel plating solution in ammonia-free environmental protection, the steps include: dissolving nickel sulfate and organic acid in water, adding sodium hypophosphite, sodium acetate, heat-stable lactic acid, wetti...
Embodiment 2
[0050] Embodiment 2 provides a kind of non-ammonia environment-friendly phosphorous electroless nickel plating solution and its preparation method, by weight, including 50 parts of heat stable grade lactic acid, 730 parts of nickel sulfate, 80 parts of organic acid, 45 parts of sodium acetate, 155 parts of sodium phosphate, 0.05 parts of wetting agent, and 0.11 parts of intermediate.
[0051] The heat-stable lactic acid is 88% lactic acid;
[0052] The organic acid is a mixture of 2-hydroxysuccinic acid and succinic acid; the 2-hydroxysuccinic acid is 50wt% of the organic acid;
[0053] Described wetting agent is sodium 2-ethylhexyl sulfate;
[0054] The intermediate is butynediol diethoxy ether.
[0055] The preparation method of the phosphorous electroless nickel plating solution in the ammonia-free environmental protection is the same as that in Example 1.
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