A kind of water-based concrete hydration temperature rise inhibitor and preparation method thereof
A concrete and inhibitor technology, applied in the field of building materials, can solve problems such as difficulty in making completely water-soluble products or aqueous solutions, and difficulty in controlling molecular weight
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Embodiment 1
[0017] Add 18g of glucose and 0.08g of sodium hydroxide into the autoclave, heat it to 180°C after vacuuming, slowly introduce 968g of ethylene oxide, and control the pressure during the whole process to not exceed 0.4MPa. After the reaction, polyether 1 is obtained. Add 10 g of diethanolamine and 40 g of an aqueous solution containing 10 g of aluminum fluoride trihydrate to 50 g of polyether 1, and stir evenly to obtain the water-based concrete hydration temperature rise inhibitor 1.
Embodiment 2
[0019] Add 34.2g of sucrose and 1.12g of potassium hydroxide into the autoclave, heat it to 200°C after vacuuming, slowly introduce 4.4g of ethylene oxide, and control the pressure during the whole process to not exceed 0.4MPa. After the reaction, polyether 2 is obtained. Add 5 g of diethanolamine and 45 g of an aqueous solution containing 5 g of magnesium fluorosilicate to 50 g of polyether 2, and stir evenly to obtain water-based concrete hydration temperature rise inhibitor 2.
Embodiment 3
[0021] Add 18.2g of mannitol and 0.24g of sodium hydride into the autoclave, heat it to 120°C after vacuuming, slowly introduce 100g of ethylene oxide, and control the pressure during the whole process to not exceed 0.4MPa. After the reaction, polyether 3 is obtained. Add 5 g of diethanolamine, 5 g of triisopropanolamine and 10 g of water to 80 g of polyether 3, and stir evenly to obtain water-based concrete hydration temperature rise inhibitor 3.
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