Seawater desalination membrane and preparation method and application thereof
A fossil and water solution technology, applied in chemical instruments and methods, seawater treatment, general water supply saving, etc., can solve the problems of poor chemical resistance, short life, low filtration effect, etc., and achieve the effect of good practicability and high efficiency
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Embodiment 1
[0019] Embodiment 1: Preparation of seawater desalination membrane
[0020] 1) The aqueous solution of graphene oxide, CdS, Fe 2 The aqueous solution of Cl is uniformly mixed; the volume mass concentration of the graphene oxide aqueous solution is 50 mg / L, and the volume mass concentration of the CdS aqueous solution is 5 mg / L; 2 The volume concentration of the aqueous solution of Cl is 10mg / L; graphene oxide, CdS, Fe 2 The mass ratio of Cl is 1:0.15:0.02, stir evenly;
[0021] 2) Using a nano-alumina membrane with an average pore size of 50 nanometers as a template, the above solution is dehydrated under negative pressure by vacuum filtration, and filled into the nanopores in the alumina membrane;
[0022] 3) Dry the composite film at 40°C for 24 hours;
[0023] 4) After irradiating with ultraviolet light for 12 hours, the divalent Fe just disappeared completely by XPS measurement, and the light was stopped to finally obtain the seawater desalination membrane.
[0024] Pr...
Embodiment 2
[0025] Embodiment 2: Preparation of seawater desalination membrane
[0026] 1) The aqueous solution of graphene oxide, CdS, Fe 2 The aqueous solution of C is uniformly mixed; the aqueous solution volume concentration of graphene oxide is 5mg / L, and the aqueous solution volume concentration of CdS is 10mg / L; 2 The volume concentration of the aqueous solution of Cl is 30mg / L; graphene oxide, CdS, Fe 2 The mass ratio of Cl is 1:0.2:0.03, stir evenly;
[0027] 2) Using a nano-alumina membrane with an average pore size of 70 nanometers as a template, the above solution is dehydrated under negative pressure by vacuum filtration, and filled into the nanopores in the alumina membrane;
[0028] 3) Dry the composite film at 40°C for 24 hours;
[0029] 4) After irradiating with ultraviolet light for 15 hours, it was measured by XPS that the divalent Fe just disappeared completely, and the light was stopped to finally obtain a seawater desalination film with a thickness of 100 nanomete...
Embodiment 3
[0031] Embodiment 3: Preparation of seawater desalination membrane
[0032] 1) The aqueous solution of graphene oxide, CdS, Fe 2 The aqueous solution of C is uniformly mixed; the volume mass concentration of the aqueous solution of graphene oxide is 25mg / L, and the volume mass concentration of the aqueous solution of CdS is 20mg / L; 2 The volume concentration of the aqueous solution of Cl is 20mg / L; graphene oxide, CdS, Fe 2 The mass ratio of Cl is 1:0.1:0.03, stir evenly;
[0033] 2) Using a nano-alumina membrane with an average pore diameter of 80 nanometers as a template, the above solution is dehydrated under negative pressure by vacuum filtration, and filled into the nanopores in the alumina membrane;
[0034] 3) Dry the composite film at 40°C for 24 hours;
[0035] 4) After irradiating with ultraviolet light for 17.5 hours, it was measured by XPS that the divalent Fe just disappeared completely, and the light was stopped, and finally a seawater desalination film with a...
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