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Electrocoppering plating solution and electrocoppering method

A technology of electroplating copper and plating solution, which is applied in the field of electroplating copper plating solution and electroplating copper, which can solve the problems that the copper plating layer affects the application of electroplating copper, the research on the surface performance of the copper plating layer, and the poor surface performance of the plating layer, etc., so as to shorten the electroplating time , The copper plating layer is bright and smooth, and the effect of improving the surface performance

Active Publication Date: 2020-05-15
GUANGZHOU SANFU NEW MATERIALS TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, this patent only studies the deep plating ability, and does not study the surface properties of the copper plating layer, and the surface properties of the copper plating layer will affect the application of electroplating copper
[0005] Therefore, there are generally technical defects in the prior art such as the coating is not bright, not smooth, poor adhesion or even decopper, and poor surface performance of the coating during high current density electroplating.

Method used

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  • Electrocoppering plating solution and electrocoppering method
  • Electrocoppering plating solution and electrocoppering method
  • Electrocoppering plating solution and electrocoppering method

Examples

Experimental program
Comparison scheme
Effect test

test approach 1

[0053] (1) Test method 1: On the copper-plated workpiece, use the tip of a knife to draw parallel or staggered scratches that reach the base (forming a 1mm×1mm square), and then paste it with 3M adhesive tape and tear it off. The coating will not be damaged. Bubble shedding is qualified;

test approach 2

[0054] (2) Test method 2: use a file to file the edge of the plated piece, if the edge of the plated piece does not bubble or only 1mm on the edge when filing 2 Peeling within the range is qualified;

test approach 3

[0055] (3) Test method 3: keep the plated parts at 260°C for 1 hour, take them out and quench them in cold water, and repeat 10 times if no peeling and peeling of the plating layer is found, it is qualified.

[0056] The experimental results are shown in Table 2.

[0057] Table 2 Copper coating adhesion test results

[0058]

[0059]

[0060] As can be seen from Table 2, the copper plating layer formed on the workpiece surface by the electroplating copper plating solution provided by the present invention has good adhesion.

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PUM

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Abstract

The invention belongs to the technical field of electroplating, and particularly relates to an electrocoppering plating solution and an electrocoppering method. The electrocoppering plating solution is composed of copper sulfate pentahydrate, sulfuric acid, chloridions, a brightener, a leveling agent, lauryl L-Arginine ethyl ester dihydrochloride, deionized water and other components. The electrocoppering method comprises the four steps of surface treatment, electrocoppering plating solution preparing, electroplating and drying. By means of the electrocoppering plating solution, electrocoppering can be carried out under the high-density current, a coppered layer of an obtained coppered workpiece is bright and smooth, adhesive force is good, the electroplating time of the low current density under the same condition can be shortened, work efficiency can be improved, and cost can be saved. The formula components of the electrocoppering plating solution are simple, the electrocoppering method is easy to achieve, and industrialization can be achieved easily.

Description

technical field [0001] The invention belongs to the technical field of electroplating, and in particular relates to a copper electroplating bath and a copper electroplating method. Background technique [0002] In recent years, people have higher and higher requirements for electronic equipment. While ensuring good performance, they are required to be smaller and lighter. The key to this is to ensure that the thickness of the copper plating layer is uniform and combined with the substrate. Strong, good conductivity and ductility, with a certain brightness and leveling properties. [0003] Acid copper plating has important applications in the electronics industry, especially in the manufacture of printed circuit boards and semiconductors. The composition of electroplating copper plating solution (including the content of copper ions, sulfuric acid, chloride ions, additives, etc.) and process conditions will affect the discharge and electrocrystallization process of copper io...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C25D3/38C25D5/34
CPCC25D3/38C25D5/34
Inventor 邓正平田志斌包志华陈国琳
Owner GUANGZHOU SANFU NEW MATERIALS TECH
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