Method for preparing TC21 titanium alloy gradient structure with high strength and toughness
A TC21, gradient microstructure technology, applied in the field of alloy materials, can solve the problems of difficulty in preparing small samples, complex preparation process, and difficult operation, and achieve the effect of large-scale industrial promotion value, simple operation, and simple equipment.
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[0038] Example 1
[0039] (1) Select a TC21 titanium alloy plate sample with a length of about 80mm, and polish the surface of the plate titanium alloy sample with metallographic sandpaper; then use anhydrous ethanol to wet the absorbent cotton to wipe the sample, and dry it for later use, such as figure 1 Shown
[0040] (2) Connect the plate-shaped sample to the positive and negative copper plate electrodes of the pulse power supply and put it into the glove box;
[0041] (3) Vacuum the glove box with a vacuum of 4KPa, then fill the glove box with an argon atmosphere and keep the pressure at 80KPa to prevent the sample from being oxidized;
[0042] (4) Turn on the pulse power, turn on the pulse power switch, adjust the pulse voltage to 67V, pulse current to 78A, and pulse frequency to 550Hz. The heating time is 1 minute, and the real-time temperature is measured with an infrared thermometer, kept at 1000°C for 5 minutes, and then air-cooled to room temperature;
[0043] (5) After roug...
Example Embodiment
[0045] Example 2
[0046] (1) Select a TC21 titanium alloy rod-shaped sample with a diameter of 11mm and a length of about 80mm, which is first processed into a rod shape by a lathe, and then the surface of the sample is polished with metallographic sandpaper; then the sample is moistened with absolute ethanol to wipe the sample. And dry for later use, such as Figure 4 Shown
[0047] (2) Connect the sample to be heat-treated with the positive and negative copper plate electrodes of the pulse power supply and put it into the glove box;
[0048] (3) Vacuum the glove box with a vacuum of 4KPa, then pass an argon atmosphere into the glove box and keep the pressure at 80KPa to protect the sample to be heat-treated and prevent oxidation;
[0049] (4) Turn on the power and turn on the pulse power switch. Adjust the pulse voltage to 75V, pulse current to 80A, and pulse frequency to 600Hz. The heating time is 1.5 minutes, and the real-time temperature is measured with an infrared thermomete...
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