A harmless amino acid-containing aqueous solution of dead livestock and poultry and its preparation method
A technology for harmless treatment of sick and dead livestock and poultry, applied in the field of harmless amino acid-containing aqueous solution of sick and dead livestock and poultry and its preparation, can solve the problems of low amino acid content, difficult separation of oil and water, and difficult separation of water slag, so as to reduce the content of suspended solids , solve the problem of excessive waste water and improve storage stability
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Embodiment 1
[0014] A harmless amino acid-containing aqueous solution of dead livestock and poultry, the preparation method of which comprises the following steps:
[0015] (1), Weigh 10 parts of ferrous acetate, 23 parts of urea, 16.5 parts of ammonium carbonate and 18 parts of clear water and add them to the reaction kettle, the stirring speed is 120r / min, and the system temperature is maintained at 87 °C for 35 minutes under closed stirring reaction. The temperature of the reaction kettle was raised to 110°C and the reaction was sealed for 25 minutes, and the temperature of the reaction kettle was lowered to room temperature to obtain the iron ammonia complex;
[0016] (2) Weigh 100 parts of raw meal and add it to the reactor, maintain the system temperature at 145 ° C and 0.6 MPa for 40 minutes in closed reaction, add 7 parts of concentrated sulfuric acid and 9 parts of water into the reactor, and the stirring speed is 20r / min, maintain the system temperature at 110°C and 0.2MPa and s...
Embodiment 2
[0018] A harmless amino acid-containing aqueous solution of dead livestock and poultry, the preparation method of which comprises the following steps:
[0019] (1), Weigh 10 parts of ferrous acetate, 7 parts of urea, 9 parts of ammonium carbonate and 13 parts of clear water and add them to the reaction kettle, the stirring speed is 120r / min, and the system temperature is maintained at 75 ° C for 35 minutes under closed stirring reaction. The temperature of the reaction kettle was raised to 110°C and the reaction was sealed for 25 minutes, and the temperature of the reaction kettle was lowered to room temperature to obtain the iron ammonia complex;
[0020] (2) Weigh 100 parts of raw meal and add it to the reaction kettle, keep the system temperature at 125 °C and 3 MPa for closed reaction for 25 minutes, add 5 parts of concentrated sulfuric acid and 5 parts of water into the reaction kettle, and the stirring speed is 15r / min , maintain the system temperature at 105°C and 0.01M...
Embodiment 3
[0022] A harmless amino acid-containing aqueous solution of dead livestock and poultry, the preparation method of which comprises the following steps:
[0023] (1), Weigh 10 parts of ferrous acetate, 36 parts of urea, 32 parts of ammonium carbonate and 27 parts of clear water and add them to the reaction kettle, the stirring speed is 120r / min, and the system temperature is maintained at 105 °C for 35 minutes under closed stirring reaction. The temperature of the reaction kettle was raised to 110°C and the reaction was sealed for 25 minutes, and the temperature of the reaction kettle was lowered to room temperature to obtain the iron ammonia complex;
[0024] (2) Weigh 100 parts of raw meal and add it to the reactor, maintain the system temperature at 165 °C and 0.1 MPa for 50 minutes in closed reaction, add 35 parts of concentrated sulfuric acid and 40 parts of water into the reactor, and the stirring speed is 60r / min, maintain the system temperature at 130°C and 0.9MPa and s...
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