Preparation method of ammonium nonanoate weeding emulsion in water
A technology of ammonium pelargonate and water emulsion, applied in the field of pesticides, can solve the problems of residual poisonous phytotoxicity, increase of drug-resistant weed population, reduction of next crop yield, etc., and achieves the effect of broad development prospect, quick effect and enhanced permeability
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[0026] The invention provides a preparation method of ammonium pelargonic acid weed-killing water emulsion, which uses plant-source pelargonic acid mother liquor as a raw material, and includes the following steps: S1: Add pelargonic acid and ammonia water into a metering tank respectively, and first put part of pelargonic acid into a reaction kettle , and drip ammonia water into the reaction kettle to keep the reaction evenly bubbling; then add water and the remaining nonanoic acid to the reaction kettle, and continue to drop ammonia water to obtain ammonium nonanoate; S2: prepare through step S1 Add emulsifier, preservative, penetrating agent, thickener, antifreeze and water to the obtained ammonium nonanoate, and stir evenly to obtain the ammonium nonanoate weeding water emulsion.
[0027] As a preferred embodiment, it includes the following steps: S1: Add pelargonic acid and ammonia water into the metering tank at a mass ratio of 1:0.5-1:1.5, and first put pelargonic acid f...
Embodiment 1
[0032] The preparation method of ammonium nonanoate weeding water emulsion comprises the following steps:
[0033]S1: Add nonanoic acid (99%) and ammonia water (25-28%) into the metering tank respectively, first put 84kg of nonanoic acid to be reacted into a 1000L reactor, turn on the temperature control of the reactor, and control the reaction temperature to 60°C. Start stirring and the rotating speed is 100rpm, and the flow rate of 2kg / min ammonia water is added dropwise with 80kg of ammonia water to keep the reaction evenly bubbling; then add 80kg of water to the reaction kettle, keep the stirring time for 20min, add the remaining 84kg of nonanoic acid, and continue Add dropwise the remaining 80kg of ammonia water until the pH of the reaction system is 8, stop stirring to obtain ammonium nonanoate;
[0034] S2: Add agricultural milk 1602#9.84kg, potassium sorbate 492g, agricultural organic silicon 6kg, magnesium aluminum silicate 2.46kg, glycerol 4.92kg to the ammonium nona...
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