Synthesis method of nitrogen-doped carbon-coated Cu/TiO2 interface structure
A synthesis method and interface structure technology, which are applied in chemical instruments and methods, chemical/physical processes, catalyst activation/preparation, etc., to achieve good application prospects and high photocatalytic activity.
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[0024] Step 1: Synthesis of heterometallic cluster precursors.
[0025] Copper(I) chloride (49.5 mg, 0.5 mmol), 1,5-pentanedioic acid (25.5 mg, 0.2 mmol) and benzoic acid (305.5 g, 2.5 mmol) were dissolved in acetonitrile (5 mL) and treated by sonication Mixing and standing at room temperature gave a clear solution. Then acetic acid (5 μL) and Ti(OiPr) 4 (0.25mL, 0.75mmol) was added to the above mixed solution. The above mixed solution was transferred to a polytetrafluoroethylene autoclave, heated to the target reaction temperature of 80° C. and the required reaction time of 33 h. After slow cooling to room temperature, the heterometallic cluster precursor was obtained. figure 1 a and 1b are crystal structure diagrams of the heterometallic cluster precursor prepared in this example observed from two different directions. Lattice guest CH is removed for clarity 3 CN. Copper: purple, titanium: cyan, oxygen: red, carbon: black, 1c is the X-ray powder diffraction pattern (XR...
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