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Xinjunan complex as well as preparation method and application thereof

A technology of caprylostrobin and complexes, which is applied in the field of caprystrobin complexes and their preparation, can solve the problems of restricting the widespread application, flocculation, precipitation and the like of caprystrobin, so as to improve the applicability of mixing and improve the The effect of bactericidal activity

Active Publication Date: 2020-08-07
SHANDONG VICOME GREENLAND CHEMICAL CO LTD
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  • Abstract
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  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Cycloprodil is a cationic type, which has great limitations in the preparation of preparations, especially compound preparations. In the actual application process, it is also prone to flocculation and precipitation when mixed with other products in tanks, which has become the main factor restricting the large-scale application of octoprodil. factor

Method used

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  • Xinjunan complex as well as preparation method and application thereof
  • Xinjunan complex as well as preparation method and application thereof
  • Xinjunan complex as well as preparation method and application thereof

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0022] Weigh octoprodil and zinc sulfate heptahydrate in the ratio of mass ratio 3:4, mix the two under the condition of water (the amount of water is 2 times of the mass sum of the former two), continue to stir at a speed of 50rpm, and react The complexation was completed after 2 hours. After vacuum filtration and 4 hours of heating and drying, the octocalid-zinc complex (complex 1) was obtained.

Embodiment 2

[0024] Weigh octoprodil and zinc acetate dihydrate according to the mass ratio of 1:1, mix the two under the condition of water (the amount of water is 1 times of the mass sum of the former two), and under the condition of 50 ℃, the Stir continuously at a high speed, and the complexation is completed after 2 hours of reaction. After 24 hours of freeze-drying, the complex of octocalid-zinc (complex 2) is obtained.

Embodiment 3

[0026] Weigh octoprodil and copper sulfate pentahydrate according to the ratio of mass ratio 0.87:1, mix the two under the condition of water (the amount of water is 3 times of the mass sum of the former two), continue to stir at a speed of 30rpm, and react After 2 hours, the complexation was completed. After pressure filtration and 4 hours of heating and drying, the octocalid-copper complex (complex 3) was obtained.

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Abstract

The invention provides a Xinjunan complex as well as a preparation method and application thereof, and belongs to the technical field of pesticides; the Xinjunan complex is prepared from Xinjunan andmetal ions; the metal ions are one or a combination of more of iron, zinc, copper, manganese, calcium, magnesium and silver. The invention has the beneficial effects that the bactericide Xinjunan is complexed with metal ions, so that the prepared Xinjunan complex has sterilization and nutrition functions at the same time, the sterilization activity of Xinjunan is improved, and meanwhile, the mixing applicability and stability of Xinjunan are improved.

Description

technical field [0001] The present invention relates to the technical field of pesticides, in particular to a octoprodil complex and a preparation method and application thereof. The octoprodil complex is used as an active ingredient for sterilization and plant nutrition. Background technique [0002] Cycloprodil is an alkylpolyamine compound, and its nature is diethylenetriamine substituted by di-n-octyl group. It has broad-spectrum antibacterial activity and is currently widely used as a bactericidal ingredient in agricultural planting, breeding, and industrial anticorrosion. Great market potential. Acetate of octoprodil can produce ionization in aqueous solution and adsorb various pathogens that are usually negatively charged, thereby inhibiting the reproduction of fungi, bacteria, and viruses, coagulating the protein of bacteria, denaturing the enzyme system of bacteria, and forming polymers. The thin film blocks the ion channels of this part of microorganisms, causing ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C07C211/65C07C209/00A01N33/04A01N55/02A01P1/00A01P3/00C05G3/60
CPCC07C211/65C07C209/00A01N33/04A01N55/02C05G3/60C05D9/02
Inventor 徐梁王永星姜万年张灿光董金居赵宪府朱立军
Owner SHANDONG VICOME GREENLAND CHEMICAL CO LTD
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