Novel sweet inhibitor co-crystal and preparation method thereof
A new technology of co-crystallization, applied in the field of food additives, can solve problems such as moisture absorption and deterioration, achieve the effects of ensuring quality and mass production, improving caking problems, and solving safety problems
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Embodiment 1
[0020] A preparation method of a novel sweetener co-crystal, which includes the following steps: a solution containing glucose is heated and concentrated under reduced pressure at 120°C to obtain a supersaturated solution with a solid content of 83%; in a constant temperature water bath at 75°C , While stirring (stirring speed 1000rpm) while adding sweetener (which consists of 2-(4-methoxyphenoxy) sodium propionate, triterpene glycoside and alkali metal heptyl sulfonate in a weight ratio of 4:2 :1 Mixing composition), then add the above supersaturated solution, spin crystallization at high speed at 1500rpm, centrifuge at 9000rpm centrifugal speed for 20min to remove water, and dry at 45℃ for 12h to obtain co-crystal containing sweetener. Wherein, the weight ratio of the glucose to the sweetener is 1:1.
Embodiment 2
[0022] The difference between this embodiment and embodiment 1 is that after adding the supersaturated solution, it also includes the step of adding seed crystals.
[0023] The seed crystals are prepared by the following method: preparing an aqueous glucose suspension at room temperature, adding a sweetener (the weight ratio of sweetener to glucose is 1:1) while stirring, and heating to 75°C to obtain a uniform solution; Cool to 35°C, precipitate, wash, and dry to obtain seed crystals.
Embodiment 3
[0025] A preparation method of a novel sweetener co-crystal, which includes the following steps: a solution containing glucose is heated and concentrated under reduced pressure at 125°C to obtain a supersaturated solution with a solid content of 85%; in a constant temperature water bath at 80°C , While stirring (stirring speed 1500rpm) while adding sweetener (which consists of 2-(4-methoxyphenoxy) sodium propionate, triterpene glycoside and alkali metal heptyl sulfonate in a weight ratio of 5:3 : 2 mixing composition), then add the above supersaturated solution, spin crystallization at 1800 rpm, centrifuge at 10000 rpm for 30 min to remove water, and dry at 60 ℃ for 12 h to obtain co-crystals containing sweetener. Wherein, the weight ratio of the glucose to the sweetener is 1:2.
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