The invention discloses a piglet and calf amniotic fluid adsorbent and a preparation method thereof. The adsorbent consists of the following raw materials by weight: 40 to 48kg of montmorillonite, 1 to 2kg of boric acid, 2 to 3kg of zinc oxide, 30 to 40kg of light calcium carbonate, 0.5 to 1kg of potassium hydrogen persulfate, 8 to 12kg of zeolite powder, 2 to 5kg of talcpowder, 0.5 to 1kg of eucalyptus oil, 0.5 to 1kg of rosemary essential oil, 0.5 to 1kg of clove oil and 0.5 to 1kg of geranium oil. The preparation method comprises the following steps of: (1) grinding the boric acid, the potassium hydrogen persulfate and the zinc oxide for later use; (2) mixing the materials for later use and the zeolite powder, adding the eucalyptus oil, the rosemary essential oil, the clove oil and thegeranium oil, and mixing to obtain materials for later use; and (3) mixing the montmorillonite, the talcpowder and the light calcium carbonate, mixing the materials for later use, blanking, and packing into bags. The adsorbent is quickly and uniformly coated on the whole bodies of newly born piglets and calves, can quickly absorb amniotic fluid on the bodies, ensures that heat of the bodies is not diffused, is easy to fall, enhances the physique of the piglets and the calves, and improves the survival rate.