A kind of preparation method of microporous optical reflective film
An optical reflection and microporous technology, applied in optics, nonlinear optics, instruments, etc., can solve the problems of low reflectivity of reflective film, uneven foaming, and low foaming efficiency, so as to reduce manufacturing costs and benefit The effect of recycling, high reflection effect
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[0023] A preparation method of a microporous optical reflective film, in which micropores are uniformly distributed in the reflective film, and a PET type polymer reflective film is taken as an example, the preparation method comprises:
[0024] The production of PET substrates can be single-layer, double-layer or three-layer according to needs: a common method is to dry and pretreat PET slices first, then melt them by extrusion, and cast them into films. The gas-type twin-screw extruder does not need a drying device. Regarding solvents, the types of solvents that can be used include DMF (N,N-dimethylformamide), xylene, phenol, tetrachloroethane, acetone, butanone , ethanol, etc., the solvent can be used alone, or can be used after compounding as needed. In this embodiment, PET reflective film is taken as an example, and phenol+tetrachloroethane can be used as a mixed solvent. In order to make the base film and solvent quickly Compatibility occurs, the base film and the mixed ...
Embodiment 1
[0030] Taking the high molecular polymer as PET as an example, the preparation method of the microporous optical reflective film includes the following steps:
[0031] Preparation of PET base material: first dry and pretreat PET slices, the drying temperature is 150 degrees for 4 hours, and then melted by extrusion, the extrusion temperature is set at 275 degrees, the melt is transported to the hanger type die head, and from the die The slit mouth of the head flows out, and is pressed by the electrostatic adsorption system on the quenching roller to form a film. Phenol: tetrachloroethane = 7: 3 is used as the mixed solvent. In order to make the base film and the solvent quickly compatible, the above-mentioned The base film and the mixed solvent are preheated, and the preheating temperature is 75 degrees;
[0032] In order to make the stretching go smoothly, and further promote the compatibility between the solvent and the base film, the above-mentioned coated film is sent to a...
Embodiment 2
[0037] Taking the high molecular polymer as PP as an example, the preparation method of the microporous optical reflective film includes the following steps:
[0038] Preparation of PP base material: first send PP chips into the extruder for extrusion and melting, the extrusion temperature is set at 200 degrees, the melt is transported to the hanger-type die, and flows out from the slit of the die, and is electrostatically charged. The adsorption system presses the chill roll to form a film. Chloroform was chosen as the solvent. In order to make the base film and the solvent compatible quickly, the above base film and the mixed solvent can be preheated, and the preheating temperature is 50 degrees;
[0039] In order to make the stretching go smoothly, and further promote the compatibility between the solvent and the base film, the above-mentioned coated film is sent to an oven for heating, and the heating temperature is 100 degrees;
[0040] The heated film is first stretche...
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