High-temperature corrosion inhibitor for acidification
A high-temperature corrosion inhibitor and corrosion inhibition technology, applied in the direction of chemical instruments and methods, drilling compositions, etc., can solve the problems of poor compatibility between corrosion inhibitors and acid liquid systems, increased cost of corrosion inhibitors, etc., and achieve product performance Safe and reliable, reducing the risk of flammability, and convenient transportation
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[0023] Example 1
[0024] A kind of preparation method of high temperature corrosion inhibitor, its steps are as follows:
[0025] 1) Preparation of mixed solution containing aldosterone amine polycondensate: add 70 g of formaldehyde and 300 g of acetophenone into the reaction flask, then add 2 mL of 37.5 wt. The temperature was raised to 90°C at a speed of 2min / °C, kept for 4h, then dropped to room temperature and left for stratification for 4h, the lower layer of water was separated, and the upper layer product was an aldehyde-ketone polycondensate; then, at room temperature and at 0.5~1r / s 200g of polyethylene polyamine (number-average molecular weight: 3000) was added dropwise to the solution state aldehyde and ketone polycondensate under the stirring speed of When it is lowered to room temperature, the obtained product is the mixed solution containing the aldosterone amine polycondensate; after testing, the molecular weight of the aldosterone amine polycondensate in the ...
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[0027] Example 2
[0028] A kind of preparation method of high temperature corrosion inhibitor, its steps are as follows:
[0029] 1) Prepare a mixed solution containing aldosterone amine polycondensate: add 32 g of formaldehyde and 120 g of acetophenone into the reaction flask, then add 2 mL of 37.5 wt. The temperature was raised to 80°C at a speed of 2min / °C, kept for 5h, and then dropped to room temperature for 4.5h. Under the stirring speed of s, 450g of polyethylene polyamine (number average molecular weight is 4200) was added dropwise to the solution state aldehyde and ketone polycondensate. After cooling down to room temperature, the obtained product is a mixed solution containing aldosterone amine polycondensate; after testing, in the mixed solution containing aldosterone amine polycondensate, the molecular weight of aldosterone amine polycondensate is 3500;
[0030] 2) In parts by weight, 26 parts of mixed solutions containing aldosterone amine polycondensate, 4 par...
Example Embodiment
[0031] Example 3
[0032] A kind of preparation method of high temperature corrosion inhibitor, its steps are as follows:
[0033]1) Prepare a mixed solution containing aldosterone amine polycondensate: add 150 g of formaldehyde and 120 g of cyclohexanone to the reaction flask, then add 2 mL of 37.5 wt. The temperature was raised to 90°C at a speed of 2min / °C, kept for 4h, then dropped to room temperature and left for stratification for 5h, the lower layer of water was separated, and the upper layer product was an aldehyde-ketone polycondensate; then, at room temperature and at 0.5~1r / s 270g of polyethylene polyamine (number-average molecular weight: 3800) was added dropwise to the solution aldehyde and ketone polycondensate under the stirring speed of When it is lowered to room temperature, the obtained product is the mixed solution containing the aldosterone amine polycondensate; after testing, in the mixed solution containing the aldosterone amine polycondensate, the molec...
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