A natural ingredient that inhibits the synthesis of melanin and its application in cosmetics
A technology of natural ingredients and uses, applied in the direction of cosmetics, cosmetic preparations, medical preparations containing active ingredients, etc., can solve the problems of research on the activity and whitening of polysaccharide F1 without purification
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Embodiment 1
[0026] Example 1: Enzyme test
[0027] 1. Test materials
[0028] Purified polysaccharide F1 was prepared according to the above-mentioned literature method and stored at -20°C.
[0029] The purity of positive control β-arbutin is not less than 98%.
[0030] The water used in the experiment was Wahaha pure water, and the chemical reagents were all conventional reagents.
[0031] 2. Test method
[0032] Reference method (synthesis of cinnamic acid-coumarin ester analogs and study on their inhibition of tyrosinase activity, Organic Chemistry, Chin.J.Org.Chem.2020,40) Determination of purified polysaccharide F1 and positive control against tyrosine Enzyme inhibition rate:
[0033] The purified polysaccharide F1 and the positive control were respectively dissolved in 50% DMSO aqueous solution and diluted into solutions with different concentrations. After mixing 130 μL phosphate buffer solution (50 mM, pH=6.8), 10 μL tyrosinase solution (final concentration 33.3 U / mL) and 10 ...
Embodiment 2
[0039] Embodiment 2: cell test
[0040] 1. Test materials
[0041] Purified polysaccharide F1 was prepared according to the above-mentioned literature method and stored at -20°C.
[0042] Mouse melanoma B16-F10 cells were purchased from ATCC.
[0043] DMEM high glucose medium and FBS were purchased from Gibco.
[0044] 2. Test method
[0045] 1. Cell culture
[0046] Mouse melanoma B16F10 cells were incubated with DMEM high glucose medium containing 10% FBS and 1% double antibody at 37°C, 5% CO 2 , cultured and passaged under saturated humidity conditions.
[0047] 2. Determination of inhibition of melanin content
[0048]Reference method (Structure modification of curcumol and inhibition of melanin content research, natural product research and development, Nat Prod Res Dev 2020, 32), using NaOH lysis method to determine the content of melanin in cells:
[0049] B16F10 cells in the logarithmic growth phase were taken, digested to make a cell suspension, and seeded in a...
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