Preparation method for polyurethane nano zinc oxide super-hydrophobic coating

A nano-zinc oxide, super-hydrophobic coating technology, applied in polyurea/polyurethane coatings, coatings, devices for coating liquids on surfaces, etc. Loss of super-hydrophobic properties and other problems, to achieve the effects of uniform and controllable coating thickness, low equipment requirements, and simple preparation methods

Inactive Publication Date: 2020-10-30
NANCHANG HANGKONG UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] Although there are quite a few ways to prepare super-hydrophobic surfaces, the rough structure of super-hydrophobic surfaces is at the micro-nano scale and is easily damaged, resulting in the loss of super-hydrophobic properties from the surface. The size of the surface has relatively precise requirements, and the superhydrophobic preparation method with a large roughness cannot control the thickness of the coating well, which affects the application of the superhydrophobic surface.

Method used

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  • Preparation method for polyurethane nano zinc oxide super-hydrophobic coating
  • Preparation method for polyurethane nano zinc oxide super-hydrophobic coating
  • Preparation method for polyurethane nano zinc oxide super-hydrophobic coating

Examples

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Embodiment 1

[0030] The operation of this example is basically the same as that of the comparative example, except that the mixed solution is mixed with 10wt% nano-zinc oxide mixed solution, so that the obtained coating has a thickness of 150 μm and a static surface contact angle of 160°.

Embodiment 2

[0032] The operation of this example is basically the same as that of Example 1, except that the sandpaper used in the substrate pretreatment is 1500 mesh, and the polyurethane elastomer is dissolved by mechanical stirring in the mixed solution configuration, and the thickness of the coated liquid layer is 300 μm. Dithiol ethanol solution was used for hydrophobic modification, and the thickness of the obtained coating was 100 μm, and the static contact angle of the surface was 162°.

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Abstract

The invention discloses a preparation method for a polyurethane nano zinc oxide super-hydrophobic coating. The method comprises the following preparation steps: grinding a base material, cleaning andpre-treating the base material, adopting a mechanical-ultrasonic vibrating way to prepare a polyurethane mixed solution; coating a certain thickness of the polyurethane mixed solution on the surface of a base body, enabling the mixed solution to separate out and cure into a film under a high-moisture environment, cleaning and drying the film, putting the film into an alcohol solution with low-surface-energy substances to modify, and drying the film to the polyurethane nano zinc oxide super-hydrophobic coating with super-hydrophobicity. The preparation method is simple in preparation conditionand operation requirement; the prepared coating has controllable thickness, and uniform and compact surface micro-nano structure distribution; and a coating contact angle can be 160 degrees after thelow-surface-energy substances are modified.

Description

technical field [0001] The invention relates to the technical field of preparation of superhydrophobic materials, in particular to a method for preparing a polyurethane nanometer zinc oxide superhydrophobic coating. Background technique [0002] A superhydrophobic surface refers to a surface with a static contact angle of water droplets greater than 150° and a rolling angle of less than 10°. This type of surface was first discovered on lotus leaves. Through the interaction of special micro-nano structures and low surface energy, surface water droplets Not easy to apply. Superhydrophobic surfaces also exhibit excellent properties such as self-cleaning, anti-corrosion, anti-icing, and anti-fog in different environments, so they have great application prospects in the fields of construction, instrumentation, and scientific research. [0003] Although there are quite a few ways to prepare super-hydrophobic surfaces, the rough structure of super-hydrophobic surfaces is at the mi...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B05D7/24B05D5/00B05D7/14B05D7/00B05D3/12C09D175/04C09D7/61
CPCB05D7/24B05D5/00B05D7/14B05D7/00B05D3/12C09D175/04C09D7/61B05D2202/15B05D2202/45B05D2202/25B05D2202/30B05D2203/35B05D2252/00C08K2201/011C08K2003/2296
Inventor 薛名山计俞伟李娜罗一丹殷祚炷洪珍谢婵徐吉林
Owner NANCHANG HANGKONG UNIVERSITY
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