Aluminum-copper alloy powder for 3D printing and preparation method thereof

An aluminum-copper alloy, 3D printing technology, applied in the field of 3D printing, can solve problems such as unfavorable large-scale popularization and application, low rare earth element content, poor product performance, etc., and achieve improved SLM performance, uniform distribution of alloy components, and stable performance. Effect

Inactive Publication Date: 2020-11-03
TONGJI UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The aluminum-silicon alloy prepared by SLM technology has a maximum tensile strength of about 450MPa, an elongation of about 4%, moderate tensile strength and low elongation
2xxx, 7xxx and other series of aluminum alloys with higher strength and better ductility often produce a large number of cracks during SLM processing, resulting in cracks, resulting in poor product performance, which is far from being comparable to conventionally manufactured aluminum alloys. Therefore, Difficult to fabricate by SLM technology
[0006] 2xxx aluminum alloys have high specific strength, excellent fatigue properties and good damage resistance, and are widely used in aerospace and other fields, but the aluminum-copper alloys prepared by traditional methods need to undergo complex post-processing (heat treatment, cold working, hot working and / or stretching), in order to obtain optimized properties, such as high strength, etc.
However, the content of rare earth elements is low and the price is expensive, which is not conducive to large-scale promotion and application

Method used

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Examples

Experimental program
Comparison scheme
Effect test

preparation example Construction

[0033] The present invention provides a method for preparing aluminum-copper alloy powder for 3D printing, which includes the following steps:

[0034] After heating and melting the aluminum-copper alloy raw materials, make them fully mixed and uniform;

[0035] Use high-speed compressed airflow to impact the molten aluminum-copper alloy flow, break it into aerosolized particles, and after cooling, obtain the aluminum-copper alloy powder produced by the gas atomization technology;

[0036] After gas atomization, the aluminum-copper alloy powder is sieved to obtain aluminum-copper alloy powder within the required particle size range for 3D printing;

[0037] The proportion of aluminum and copper in the aluminum-copper alloy raw materials meets the requirements of the final aluminum-copper alloy powder used for 3D printing: Cu content is 1.00%wt-8.00%wt, Mg content is 0.10%wt-4.00%wt, and Si content is 0.05% wt-3.00%wt, Mn content is 0.04%wt-2.50%wt, Zr content is 0.01%wt-3.00%wt, and t...

Embodiment 1

[0050] According to Cu content is 3.97%wt, Mg content is 1.85%wt, Si content is 1.25%wt, Mn content is 0.72%wt, Zr content is 0.87%wt, and the rest is Al, the alloy raw materials are respectively taken for vacuum melting at 810℃ After holding for half an hour, use the Hartmann-Laval vacuum atomization technology developed by Tongji for atomization (it uses a supersonic atomizing nozzle that combines laval and hartmann structures, and a supersonic atomizing nozzle that combines laval and hartmann structures The specific structure can refer to the supersonic atomization nozzle fusion laval and hartmann disclosed in Chinese patent CN201410553284.7), the atomizing gas is high-purity argon, the gas pressure during atomization is 2.5MPa, and the tight coupling method is adopted to ensure The outlet negative pressure is 0.7kPa, and the first-order resonance gas frequency is 100kHz. After the gas is atomized, the powders with a particle size of 10-60 μm are screened out by cyclone clas...

Embodiment 2

[0052] This embodiment provides a method for preparing aluminum-copper alloy powder for 3D printing, including the following steps:

[0053] The aluminum-copper alloy raw materials (the ratio of aluminum-copper in the aluminum-copper alloy raw materials to meet the final aluminum-copper alloy powder used for 3D printing: Cu content is 4.70%wt, Mg content is 2.00%wt, Si content is 1.86%wt, The content of Mn is 0.92%wt, the content of Zr is 1.50%wt, and the rest is Al) After heating and melting at 750°C, it is fully mixed and uniform;

[0054] Adopt high-speed compressed air flow (argon gas, gas pressure is 5.0MPa, adopt a tight coupling method to ensure that the negative pressure at the outlet is 1.0kPa) impact the molten aluminum-copper alloy flow, break it into aerosolized particles, and pass through after cooling Aluminum-copper alloy powder made by gas atomization technology;

[0055] After gas atomization, the aluminum-copper alloy powder is sieved by cyclone classification siev...

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Abstract

The invention relates to a preparation method of aluminum-copper alloy powder for 3D printing, and belongs to the technical field of 3D printing of metal powder. After being heated and molten, aluminum-copper alloy raw materials are fully mixed evenly; aluminum-copper alloy powder is prepared by a gas atomization technology; after gas atomization, the aluminum-copper alloy powder is sieved to obtain the aluminum-copper alloy powder for 3D printing within the required particle size range; and the proportion of aluminum and copper in the aluminum-copper alloy raw materials meets the aluminum-copper alloy powder for 3D printing, specifically, the Cu content is 1.00%wt to 8.00%wt, the Mg content is 0.10%wt to 4.00%wt, the Si content is 0.05%wt to 3.00%wt, the Mn content is 0.04%wt to 2.50%wt,the Zr content is 0.01%wt to 3.00%wt, and the balance is Al. The strength of a sample prepared by selective laser melting (SLM) of the aluminum-copper alloy powder is equal to that of an SLM aluminum-silicon alloy, but the elongation of the sample is obviously higher than that of the common SLM aluminum-silicon alloy, the using demands for an aluminum alloy in most cases can be met, the complex post-treatment process of the malleable aluminum alloy is reduced, and energy and the cost are saved.

Description

Technical field [0001] The invention belongs to the technical field of 3D printing, and particularly relates to an aluminum copper alloy powder used for 3D printing and a preparation method thereof. Background technique [0002] 3D printing is a manufacturing technology that uses three-dimensional model data to obtain products with complex shapes through layers of accumulation. Compared with the traditional preparation methods of plastics, ceramics, metals and alloys, and composite materials, 3D printing technology has a series of advantages such as the ability to prepare high-precision and complex-shaped products, saving raw materials, and saving costs, and has good application prospects. Currently commonly used 3D printing methods include direct three-dimensional printing technology (3DP), selective laser melting technology (SLM), stereo light curing technology (SLA), fused deposition technology (FDM), etc., among which selective laser melting technology (SLM) It is widely use...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B22F9/08B22F1/00B22F3/105C22C21/08C22C21/14C22C21/16B33Y70/00
CPCB22F9/082C22C21/14C22C21/16C22C21/08B33Y70/00B22F2009/0824B22F2009/0892B22F1/065Y02P10/25
Inventor 尹春月严鹏飞严彪
Owner TONGJI UNIV
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