Water-soluble solid etching reagent for anti-dazzle high-aluminum glass, and etching process for high-aluminum glass

A high-alumina glass and solid reagent technology, applied in the direction of surface etching compositions, chemical instruments and methods, etc., can solve the problems of poor stability of etching liquid, difficult recycling, strong volatility, etc., to improve etching effect and facilitate storage and transportation, easy to operate

Pending Publication Date: 2020-11-10
海南海控特玻科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

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Problems solved by technology

Although the production method of this invention is simple, easy to operate, and saves manpower, it still needs to add reagents such as hydrochloric acid and sulfuric acid, which belong to the anti-glare reagent formula that needs to add acid solvents. Using these strong acids will pollute the environment, and hydrochloric acid is highly volatile. , resulting in poor stability of the etchant, making it difficult to be recycled

Method used

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  • Water-soluble solid etching reagent for anti-dazzle high-aluminum glass, and etching process for high-aluminum glass
  • Water-soluble solid etching reagent for anti-dazzle high-aluminum glass, and etching process for high-aluminum glass
  • Water-soluble solid etching reagent for anti-dazzle high-aluminum glass, and etching process for high-aluminum glass

Examples

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Effect test

Embodiment 1

[0044] A water-soluble anti-glare high-alumina glass etching solid reagent comprises the following raw materials in parts by weight: 15 parts of ammonium bifluoride, 30 parts of citric acid, 10 parts of ammonium sulfate, 2 parts of potassium hydrogen fluoride, 3 parts of titanium dioxide, and 5 parts of D-sorbitol.

[0045] The high alumina glass etching process includes the following steps:

[0046] (1) Weigh raw materials according to the above weight ratio: 15 parts of ammonium bifluoride, 30 parts of citric acid, 10 parts of ammonium sulfate, 2 parts of potassium bifluoride, 3 parts of titanium dioxide, 5 parts of D-sorbitol, and add 300 parts of ultrapure water , mix at room temperature, stir evenly at 300r / min, put it into a polytetrafluoroethylene container, and age it ultrasonically at 25°C for 8 hours to prepare an etching solution;

[0047] (2) After cleaning the pre-etched flat high-alumina glass with a surfactant, place it in deionized water mixed with absolute eth...

Embodiment 2

[0051] A water-soluble antiglare high-alumina glass etching solid reagent, the raw materials of which are: 35 parts by weight of ammonium bifluoride, 20 parts of citric acid, 8 parts of ammonium sulfate, 2 parts of potassium hydrogen fluoride, 3 parts of titanium dioxide, and 6 parts of microcrystalline cellulose. The raw materials were weighed according to the above parts by weight. The high alumina glass etching process of this embodiment is different from that of Embodiment 1 in that the aging time of step (1) is 12 hours, and the soaking time of step (4) is 20 minutes.

Embodiment 3

[0053]A water-soluble anti-glare high-alumina glass etching solid reagent comprises the following raw materials in parts by weight: 25 parts of ammonium bifluoride, 30 parts of citric acid, 15 parts of ammonium sulfate, 2 parts of potassium sulfate, 4.5 parts of titanium dioxide, and 5 parts of D-sorbitol. The raw materials were weighed according to the above parts by weight. The high alumina glass etching process of this embodiment is different from that of Embodiment 1 in that the aging time of step (1) is 16 hours, and the soaking time of step (4) is 30 minutes.

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Abstract

The invention provides a water-soluble solid etching reagent for anti-dazzle high-aluminum glass, and an etching process for the high-aluminum glass. The solid etching reagent comprises the followingraw materials by weight: 15-45 parts of ammonium bifluoride, 20-60 parts of citric acid, 6-15 parts of ammonium sulfate, 2-14 parts of potassium bifluoride or potassium sulfate, 1-10 parts of titaniumdioxide, and 5-50 parts of a thickener. The solid etching reagent disclosed by the invention can be dissolved in water, so strong acid and toxic organic solvents are not used; the high-alumina glasscan be well etched under the condition of normal temperature; and the prepared finished anti-dazzle high-alumina glass product can generate a good anti-dazzle effect.

Description

technical field [0001] The invention relates to the technical field of functional glass products, in particular to a water-soluble antiglare high-alumina glass etching solid reagent and a high-alumina glass etching process. Background technique [0002] At present, the anti-glare glass sold in domestic and foreign markets is generally achieved by coating the glass surface or corroding the glass surface by using hydrofluoric acid. The anti-glare glass prepared by coating method has better effect, but the process is complicated, and it is generally required to be carried out under vacuum conditions, the cost is high, and the film layer is easy to fall off when used outdoors, with poor weather resistance and abrasion resistance. Appearance, transmittance, etc. have an impact. The traditional glass etching technology uses hydrofluoric acid and concentrated sulfuric acid under elevated temperature conditions. The glass surface is corroded by hydrofluoric acid to form a frosted s...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C03C15/00C09K13/00
CPCC03C15/00C09K13/00
Inventor 姜宏李筱凡赵会峰周莉郝霞王琦潘国治
Owner 海南海控特玻科技有限公司
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