Conductive polymer, capacitor and preparation method thereof
A conductive polymer and capacitor technology, applied in the field of capacitors, can solve the problems of dedoping, poor conductivity, etc., and achieve the effects of improving conductivity, strong doping stability, and improving migration efficiency
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[0036] Another embodiment of the present invention provides a method for preparing a capacitor, comprising the following steps:
[0037] Obtain a monomer solution, which includes a compound shown in general formula 1:
[0038]
[0039] Formula 1
[0040] Wherein, Y is selected from one of NH and S; R 1 , R 2 each independently selected from H or optionally substituted linear or branched alkyl, optionally substituted cycloalkyl, optionally substituted aryl, optionally substituted aralkyl, optionally substituted alkoxy, or hydroxyl and an organic group containing at least one of carboxyl, sulfonic acid and phosphoric acid, and R 1 and R 2 At least one is an organic group containing at least one of carboxyl, sulfonic acid and phosphoric acid;
[0041] The capacitor element is impregnated in the monomer solution, the impregnated capacitor element is taken out, dried, impregnated with an oxidant solution, polymerized, sealed and assembled to obtain a capacitor.
[0042] The ...
Embodiment 1
[0059] This embodiment is used to illustrate the conductive polymer disclosed in the present invention, the capacitor and the preparation method thereof, including the following steps:
[0060] S1. Use 3,4-ethylenedioxythiophene-2'-methanesulfonic acid as the polymer monomer, use ethanol as the solvent to prepare the polymer monomer into a 25% monomer solution, and use capacitor elements to impregnate the monomer solution 2min, take out the capacitor element and dry it in an oven at 80°C for 30min, then cool to room temperature;
[0061] S2. After the above steps, the element is vacuum impregnated with 55% ferric p-toluenesulfonate ethanol oxidant solution, the vacuum degree is -0.085MPa, slowly put the capacitor element into the oxidant solution, and keep the temperature between 20-25°C time, the time is maintained for 5 minutes;
[0062] S3. After the impregnation is completed, remove the capacitor element and put it in a constant temperature and humidity box for polymeriza...
Embodiment 2
[0065] This embodiment is used to illustrate the conductive polymer disclosed in the present invention, the capacitor and the preparation method thereof, including the following steps:
[0066] S1. Use 3,4-ethylenedioxythiophene-2',3'-dimethylsulfonic acid as the polymer monomer, use ethanol as the solvent to prepare the polymer monomer into a 27% monomer solution, and use capacitor elements Immerse in the monomer solution for 2 minutes, take out the capacitor element and dry it in an oven at 90°C for 30 minutes, then cool to room temperature;
[0067] S2. After the above steps, the element is vacuum impregnated with 60% ferric p-toluenesulfonate ethanol oxidant solution, the vacuum degree is -0.09MPa, slowly put the capacitor element into the oxidant solution, and keep the temperature between 20-25°C time, the time is maintained for 5 minutes;
[0068] S3. After the impregnation is completed, remove the capacitor element and put it into a constant temperature and humidity bo...
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